2-acetamido-N-tert-butyl-2-(3-(2,4-dichlorophenethylamino)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide

Base Information

Chemical Name:2-acetamido-N-tert-butyl-2-(3-(2,4-dichlorophenethylamino)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide
CAS No.:1345673-42-8
Molecular Formula:C₂₉H₄₈BCl₂N₃O₄
Molecular Weight:584.435
Hs Code.:

Synonyms:2-acetamido-N-tert-butyl-2-(3-(2,4-dichlorophenethylamino)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide

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Chemical Property of 2-acetamido-N-tert-butyl-2-(3-(2,4-dichlorophenethylamino)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide

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Technology Process of 2-acetamido-N-tert-butyl-2-(3-(2,4-dichlorophenethylamino)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide

There total 5 articles about 2-acetamido-N-tert-butyl-2-(3-(2,4-dichlorophenethylamino)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 30067-11-9
2-(2,4-dichlorophenyl)acetaldehyde

: 2-acetamido-2-(3-aminopropyl)-N-tert-butyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide hydrochloride

: 1345673-42-8
2-acetamido-N-tert-butyl-2-(3-(2,4-dichlorophenethylamino)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide

Guidance literature:: 2,4-dichlorophenylacetaldehyde; 2-acetamido-2-(3-aminopropyl)-N-tert-butyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide hydrochloride; In dichloromethane; at 20 ℃; for 0.5h;

With sodium tris(acetoxy)borohydride; In dichloromethane;

Reference yield:

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 1345673-42-8
2-acetamido-N-tert-butyl-2-(3-(2,4-dichlorophenethylamino)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,2,2-trifluoroethanol / 72 h / 20 °C

2.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: 16 h

3.1: hydrogenchloride / ethyl acetate / 0.5 h / 20 °C

4.1: dichloromethane / 0.5 h / 20 °C

With hydrogenchloride; bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane; In dichloromethane; 2,2,2-trifluoroethanol; ethyl acetate;

Reference yield:

: 887402-83-7
(4-oxooct-7-enyl)carbamic acid tert-butyl ester

: 1345673-42-8
2-acetamido-N-tert-butyl-2-(3-(2,4-dichlorophenethylamino)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,2,2-trifluoroethanol / 72 h / 20 °C

2.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.2: 16 h

3.1: hydrogenchloride / ethyl acetate / 0.5 h / 20 °C

4.1: dichloromethane / 0.5 h / 20 °C

With hydrogenchloride; bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane; In dichloromethane; 2,2,2-trifluoroethanol; ethyl acetate;