Technology Process of 3,5-dinitro-2-pyridyl-2,3,4-tri-O-benzyl-α-L-rhamnopyranose
There total 4 articles about 3,5-dinitro-2-pyridyl-2,3,4-tri-O-benzyl-α-L-rhamnopyranose which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,6-dimethylpyridine; potassium fluoride; 18-crown-6 ether;
In
dichloromethane;
for 0.5h;
Ambient temperature;
DOI:10.1021/jm00160a025
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 85 percent / 80percent AcOH, 2N HCl / H2O / 5 h / 90 °C
2: 90 percent / 2,6-lutidine, KF, 18-crown-6 ether / CH2Cl2 / 0.5 h / Ambient temperature
With
2,6-dimethylpyridine; hydrogenchloride; potassium fluoride; 18-crown-6 ether; acetic acid;
In
dichloromethane; water;
DOI:10.1021/jm00160a025
- Guidance literature:
-
Multi-step reaction with 3 steps
1: KOH / dimethylformamide / 7 h / Ambient temperature
2: 85 percent / 80percent AcOH, 2N HCl / H2O / 5 h / 90 °C
3: 90 percent / 2,6-lutidine, KF, 18-crown-6 ether / CH2Cl2 / 0.5 h / Ambient temperature
With
2,6-dimethylpyridine; hydrogenchloride; potassium fluoride; potassium hydroxide; 18-crown-6 ether; acetic acid;
In
dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00160a025