1-(4,6-diphenyl-2-pyrimidinylcarbonyl)-4-phenyl-S-methylisothiosemicarbazide

Base Information

Chemical Name:1-(4,6-diphenyl-2-pyrimidinylcarbonyl)-4-phenyl-S-methylisothiosemicarbazide
CAS No.:476469-20-2
Molecular Formula:C₂₅H₂₁N₅OS
Molecular Weight:439.541
Hs Code.:

Synonyms:1-(4,6-diphenyl-2-pyrimidinylcarbonyl)-4-phenyl-S-methylisothiosemicarbazide

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Chemical Property of 1-(4,6-diphenyl-2-pyrimidinylcarbonyl)-4-phenyl-S-methylisothiosemicarbazide

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Technology Process of 1-(4,6-diphenyl-2-pyrimidinylcarbonyl)-4-phenyl-S-methylisothiosemicarbazide

There total 3 articles about 1-(4,6-diphenyl-2-pyrimidinylcarbonyl)-4-phenyl-S-methylisothiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 60007-26-3
1-(4,6-diphenyl-2-pyrimidinyl)-4-phenylthiosemicarbazide

: 74-88-4
methyl iodide

: 476469-20-2
1-(4,6-diphenyl-2-pyrimidinylcarbonyl)-4-phenyl-S-methylisothiosemicarbazide

Guidance literature:: With sodium methylate; In methanol; for 0.25h; Heating;

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 476469-20-2
1-(4,6-diphenyl-2-pyrimidinylcarbonyl)-4-phenyl-S-methylisothiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / ethanol / 2 h / Heating

2: 87 percent / NaOMe / methanol / 0.25 h / Heating

With sodium methylate; In methanol; ethanol;

Reference yield:

: 49676-35-9
4,6-diphenyl-2-pyrimidinecarboxylic acid

: 476469-20-2
1-(4,6-diphenyl-2-pyrimidinylcarbonyl)-4-phenyl-S-methylisothiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / ethanol / 2 h / Heating

2: 87 percent / NaOMe / methanol / 0.25 h / Heating

With sodium methylate; In methanol; ethanol;