7-benzyloxy-2-heptanone dimethylhydrazone

Base Information

• Chemical Name: 7-benzyloxy-2-heptanone dimethylhydrazone
• CAS No.: 125104-09-8
• Molecular Formula: C₁₆H₂₆N₂O
• Molecular Weight: 262.395
• Mol file: 125104-09-8.mol

Synonyms:7-benzyloxy-2-heptanone dimethylhydrazone

Chemical Property of 7-benzyloxy-2-heptanone dimethylhydrazone

Chemical Property:

Purity/Quality:

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Technology Process of 7-benzyloxy-2-heptanone dimethylhydrazone

There total 1 articles about 7-benzyloxy-2-heptanone dimethylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) → 7-benzyloxy-2-heptanone dimethylhydrazone (125104-09-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF

2: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 30 min, 2.) THF, r.t., 2 h

With n-butyllithium; sodium hydride;

DOI:10.1055/s-1989-27363

Reference yield: 69.0%

7-benzyloxy-2-heptanone dimethylhydrazone (125104-09-8) → 7-Benzyloxy-heptan-2-one (125130-47-4)

Guidance literature:

With silica gel; In tetrahydrofuran; water; at 25 ℃; for 5h;

DOI:10.1055/s-1989-27363

upstream raw materials:

benzyl bromide

Downstream raw materials:

7-Benzyloxy-heptan-2-one