(3S,4R)-3-<<(2-Nitrophenyl)sulfenyl>amino>-4-<(4-methoxyphenyl)methyl>-2-oxetanone

Base Information

Chemical Name:(3S,4R)-3-<<(2-Nitrophenyl)sulfenyl>amino>-4-<(4-methoxyphenyl)methyl>-2-oxetanone
CAS No.:157457-78-8
Molecular Formula:C₁₇H₁₆N₂O₅S
Molecular Weight:360.39
Hs Code.:

Synonyms:(3S,4R)-3-<<(2-Nitrophenyl)sulfenyl>amino>-4-<(4-methoxyphenyl)methyl>-2-oxetanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4R)-3-<<(2-Nitrophenyl)sulfenyl>amino>-4-<(4-methoxyphenyl)methyl>-2-oxetanone

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Technology Process of (3S,4R)-3-<<(2-Nitrophenyl)sulfenyl>amino>-4-<(4-methoxyphenyl)methyl>-2-oxetanone

There total 3 articles about (3S,4R)-3-<<(2-Nitrophenyl)sulfenyl>amino>-4-<(4-methoxyphenyl)methyl>-2-oxetanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 157457-75-5
(2S,3R)-2-<<(2-Nitrophenyl)sulfenyl>amino>-3-hydroxy-4-(4-methoxyphenyl)butanoic acid

: 157457-78-8
(3S,4R)-3-<<(2-Nitrophenyl)sulfenyl>amino>-4-<(4-methoxyphenyl)methyl>-2-oxetanone

Guidance literature:: With pyridine; 4-bromobenzenesulfonyl chloride; 1.) -45 deg C, 1 h, 2.) 0 deg C, 4 h;
DOI:10.1021/jo00092a025

Reference yield:

: 5703-26-4
4-Methoxyphenylacetaldehyde

: 157457-78-8
(3S,4R)-3-<<(2-Nitrophenyl)sulfenyl>amino>-4-<(4-methoxyphenyl)methyl>-2-oxetanone

Guidance literature:: Multi-step reaction with 3 steps

2: 45 percent / 1N aq. NaOH / dioxane / 0.33 h

3: 34 percent / 4-BrC₆H₄SO₂Cl, pyridine / 1.) -45 deg C, 1 h, 2.) 0 deg C, 4 h

With pyridine; sodium hydroxide; 4-bromobenzenesulfonyl chloride; In 1,4-dioxane;
DOI:10.1021/jo00092a025

Reference yield:

: 157457-72-2
(2S,3R)-2-Amino-3-hydroxy-4-(4-methoxyphenyl)butanoic acid

: 157457-78-8
(3S,4R)-3-<<(2-Nitrophenyl)sulfenyl>amino>-4-<(4-methoxyphenyl)methyl>-2-oxetanone

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / 1N aq. NaOH / dioxane / 0.33 h

2: 34 percent / 4-BrC₆H₄SO₂Cl, pyridine / 1.) -45 deg C, 1 h, 2.) 0 deg C, 4 h

With pyridine; sodium hydroxide; 4-bromobenzenesulfonyl chloride; In 1,4-dioxane;
DOI:10.1021/jo00092a025