[4-Benzyloxy-5-{5-benzyloxy-4-[5-benzyloxy-4-(5-benzyloxy-2-cyanomethoxy-4-iodo-benzyl)-2-cyanomethoxy-benzyl]-2-cyanomethoxy-benzyl}-2-(tert-butyl-diphenyl-silanyloxymethyl)-phenoxy]-acetonitrile

Base Information

• Chemical Name: [4-Benzyloxy-5-{5-benzyloxy-4-[5-benzyloxy-4-(5-benzyloxy-2-cyanomethoxy-4-iodo-benzyl)-2-cyanomethoxy-benzyl]-2-cyanomethoxy-benzyl}-2-(tert-butyl-diphenyl-silanyloxymethyl)-phenoxy]-acetonitrile
• CAS No.: 195601-80-0
• Molecular Formula: C₈₀H₇₁IN₄O₉Si
• Molecular Weight: 1387.46

Synonyms:[4-Benzyloxy-5-{5-benzyloxy-4-[5-benzyloxy-4-(5-benzyloxy-2-cyanomethoxy-4-iodo-benzyl)-2-cyanomethoxy-benzyl]-2-cyanomethoxy-benzyl}-2-(tert-butyl-diphenyl-silanyloxymethyl)-phenoxy]-acetonitrile

Chemical Property of [4-Benzyloxy-5-{5-benzyloxy-4-[5-benzyloxy-4-(5-benzyloxy-2-cyanomethoxy-4-iodo-benzyl)-2-cyanomethoxy-benzyl]-2-cyanomethoxy-benzyl}-2-(tert-butyl-diphenyl-silanyloxymethyl)-phenoxy]-acetonitrile

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Technology Process of [4-Benzyloxy-5-{5-benzyloxy-4-[5-benzyloxy-4-(5-benzyloxy-2-cyanomethoxy-4-iodo-benzyl)-2-cyanomethoxy-benzyl]-2-cyanomethoxy-benzyl}-2-(tert-butyl-diphenyl-silanyloxymethyl)-phenoxy]-acetonitrile

There total 1 articles about [4-Benzyloxy-5-{5-benzyloxy-4-[5-benzyloxy-4-(5-benzyloxy-2-cyanomethoxy-4-iodo-benzyl)-2-cyanomethoxy-benzyl]-2-cyanomethoxy-benzyl}-2-(tert-butyl-diphenyl-silanyloxymethyl)-phenoxy]-acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

benzyl bromide (100-39-0) + [4-Benzyloxy-5-{5-benzyloxy-4-[5-benzyloxy-2-cyanomethoxy-4-(2-cyanomethoxy-5-hydroxy-4-iodo-benzyl)-benzyl]-2-cyanomethoxy-benzyl}-2-(tert-butyl-diphenyl-silanyloxymethyl)-phenoxy]-acetonitrile → [4-Benzyloxy-5-{5-benzyloxy-4-[5-benzyloxy-4-(5-benzyloxy-2-cyanomethoxy-4-iodo-benzyl)-2-cyanomethoxy-benzyl]-2-cyanomethoxy-benzyl}-2-(tert-butyl-diphenyl-silanyloxymethyl)-phenoxy]-acetonitrile (195601-80-0)

Guidance literature:

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium hydride; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1021/jm970251r

Reference yield:

[4-Benzyloxy-5-{5-benzyloxy-4-[5-benzyloxy-4-(5-benzyloxy-2-cyanomethoxy-4-iodo-benzyl)-2-cyanomethoxy-benzyl]-2-cyanomethoxy-benzyl}-2-(tert-butyl-diphenyl-silanyloxymethyl)-phenoxy]-acetonitrile (195601-80-0) + Benzoic acid 3-bromomethyl-4-cyanomethoxy-phenyl ester (195601-70-8) → Benzoic acid 3-[2-benzyloxy-4-(2-benzyloxy-4-{2-benzyloxy-4-[2-benzyloxy-4-(tert-butyl-diphenyl-silanyloxymethyl)-5-cyanomethoxy-benzyl]-5-cyanomethoxy-benzyl}-5-cyanomethoxy-benzyl)-5-cyanomethoxy-benzyl]-4-cyanomethoxy-phenyl ester

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ethylene dibromide; zinc; Yield given. Multistep reaction; 1.) THF, 0-5 deg C, 2.) THF, 60 deg C, 3 h;

DOI:10.1021/jm970251r

Reference yield:

[4-Benzyloxy-5-{5-benzyloxy-4-[5-benzyloxy-4-(5-benzyloxy-2-cyanomethoxy-4-iodo-benzyl)-2-cyanomethoxy-benzyl]-2-cyanomethoxy-benzyl}-2-(tert-butyl-diphenyl-silanyloxymethyl)-phenoxy]-acetonitrile (195601-80-0) + Benzoic acid 3-(2-benzyloxy-4-bromomethyl-5-cyanomethoxy-benzyl)-4-cyanomethoxy-phenyl ester (195601-76-4) → 2-({[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl)-4-(benzyloxy)-5-[4-{4-[4-(4-{2-[(cyanomethyl)oxy]-5-(benzyloxy)benzyl}-3-(benzyloxy)-5-[(cyanomethyl)oxy]benzyl)-3-(benzyloxy)-5-[(cyanomethyl)oxy]benzyl]-3-(benzyloxy)-5-[(cyanomethyl)oxy]benzyl}...

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ethylene dibromide; zinc; Yield given. Multistep reaction; 1.) THF, 0-5 deg C, 2.) THF, 60 deg C, 1.25 h;

DOI:10.1021/jm970251r

upstream raw materials:

benzyl bromide

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