methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine

Base Information

Chemical Name:methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine
CAS No.:339193-73-6
Molecular Formula:C₂₀H₂₀N₂O₂S
Molecular Weight:352.457
Hs Code.:

methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[<i>cd</i>]indol-4-yl]-amine

Synonyms:methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine

Suppliers and Price of methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine

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Technology Process of methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine

There total 1 articles about methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 339193-69-0
methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-carbamic acid tert-butyl ester

: 339193-73-6
methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine

Guidance literature:: With toluene-4-sulfonic acid; In methanol;
DOI:10.1016/S0040-4039(01)00002-8

Reference yield: 89.0%

: 5162-44-7
1-bromo-4-butene

: 339193-73-6
methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine

: 339193-75-8
but-3-enyl-methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine

Guidance literature:: With caesium carbonate; In tetrahydrofuran; Heating;
DOI:10.1016/S0040-4039(01)00002-8

Reference yield:

: 339193-73-6
methyl-[5-methylene-1-(toluene-4-sulfonyl)-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl]-amine

: 339193-77-0
7-methyl-4-(toluene-4-sulfonyl)-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Cs₂CO₃ / tetrahydrofuran / Heating

2: 86 percent / [Mo(=NC₆H₃-2,5-di-iPr)(=CHCMe₂Ph)(OCMe(CF₃)2)2] / benzene / Heating

With [Mo(=NC₆H₃-2,5-di-iPr)(=CHCMe₂Ph)(OCMe(CF₃)2)2]; caesium carbonate; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4039(01)00002-8