(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl phenylcarbamate

Base Information

Chemical Name:(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl phenylcarbamate
CAS No.:1370723-35-5
Molecular Formula:C₂₂H₂₆BNO₄
Molecular Weight:379.264
Hs Code.:

Synonyms:(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl phenylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl phenylcarbamate

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Technology Process of (E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl phenylcarbamate

There total 3 articles about (E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 167896-49-3
(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)prop-2-en-1-ol

: 103-71-9
phenyl isocyanate

: 1370723-35-5
(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl phenylcarbamate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.201100806

Reference yield:

: 1138162-59-0
C₁₈H₂₉BO₃Si

: 1370723-35-5
(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / tetrahydrofuran; water / 0 - 20 °C

2: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; dmap; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/adsc.201100806

Reference yield:

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1370723-35-5
(E)-1-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl phenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 48 h / 100 °C / Sealed tube; Inert atmosphere

2: hydrogenchloride / tetrahydrofuran; water / 0 - 20 °C

3: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; dmap; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/adsc.201100806