octyl 2-O-benzyl-4,6-benzylidene-3-O-p-methoxybenzyl-β-D-glucopyranoside

Base Information

Chemical Name:octyl 2-O-benzyl-4,6-benzylidene-3-O-p-methoxybenzyl-β-D-glucopyranoside
CAS No.:503602-06-0
Molecular Formula:C₃₆H₄₆O₇
Molecular Weight:590.757
Hs Code.:

Synonyms:octyl 2-O-benzyl-4,6-benzylidene-3-O-p-methoxybenzyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of octyl 2-O-benzyl-4,6-benzylidene-3-O-p-methoxybenzyl-β-D-glucopyranoside

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Technology Process of octyl 2-O-benzyl-4,6-benzylidene-3-O-p-methoxybenzyl-β-D-glucopyranoside

There total 3 articles about octyl 2-O-benzyl-4,6-benzylidene-3-O-p-methoxybenzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 824-94-2
p-methoxybenzyl chloride

: 503602-04-8
octyl 2-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

: 503602-06-0
octyl 2-O-benzyl-4,6-benzylidene-3-O-p-methoxybenzyl-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1016/S0008-6215(02)00178-7

Reference yield:

: 100-39-0
benzyl bromide

: 503602-06-0
octyl 2-O-benzyl-4,6-benzylidene-3-O-p-methoxybenzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / tetrabutylammonium bromide; NaOH / CH₂Cl₂ / 48 h / 20 °C

2: 51 percent / NaH / dimethylformamide / 1 h / 20 °C

With sodium hydroxide; tetrabutylammomium bromide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(02)00178-7

Reference yield:

: 118249-73-3
octyl 4,6-O-benzylidene-β-D-glucopyranoside

: 503602-06-0
octyl 2-O-benzyl-4,6-benzylidene-3-O-p-methoxybenzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / tetrabutylammonium bromide; NaOH / CH₂Cl₂ / 48 h / 20 °C

2: 51 percent / NaH / dimethylformamide / 1 h / 20 °C

With sodium hydroxide; tetrabutylammomium bromide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(02)00178-7