(3S,3S')-3--3-(4-methoxyphenyl)-1-propanol

Base Information

Chemical Name:(3S,3S')-3--3-(4-methoxyphenyl)-1-propanol
CAS No.:159848-96-1
Molecular Formula:C₃₀H₄₄N₂O₇
Molecular Weight:544.689
Hs Code.:

(3S,3S')-3-<N-tert-butoxycarbonyl-3'-tert-butoxycarbonylamino-3'-(4-methoxyphenyl)propylamino>-3-(4-methoxyphenyl)-1-propanol

Synonyms:(3S,3S')-3--3-(4-methoxyphenyl)-1-propanol

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Chemical Property of (3S,3S')-3--3-(4-methoxyphenyl)-1-propanol

Chemical Property:

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Technology Process of (3S,3S')-3--3-(4-methoxyphenyl)-1-propanol

There total 11 articles about (3S,3S')-3--3-(4-methoxyphenyl)-1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 159848-95-0
methyl (3S,3S')-3--3-(4-methoxyphenyl)propionate

: 159848-96-1
(3S,3S')-3--3-(4-methoxyphenyl)-1-propanol

Guidance literature:: With lithium borohydride; In tetrahydrofuran; diethyl ether; for 13h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85520-4

Reference yield:

: 131690-56-7
(S)-β-amino-β-(4-methoxyphenyl)propionic acid

: 159848-96-1
(3S,3S')-3--3-(4-methoxyphenyl)-1-propanol

Guidance literature:: Multi-step reaction with 6 steps

1: 4.75 percent / 1N NaOH / tetrahydrofuran / 4 h / Ambient temperature

2: 1.20 g / K₂CO₃ / dimethylformamide / 11 h / Ambient temperature

3: 94 percent / 10percent HCl / methanol / 1 h / Ambient temperature

4: 86 percent / 1M NaBH₃CN / methanol; acetic acid; tetrahydrofuran / 15 h / 0 - 14 °C

5: 94 percent / dioxane / 14 h / Ambient temperature

6: 97 percent / 2M LiBH₄ / diethyl ether; tetrahydrofuran / 13 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; lithium borohydride; sodium cyanoborohydride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85520-4

Reference yield:

: 159848-76-7,227319-36-0
methyl (+)-(3S)-3-amino-3-(4-methoxyphenyl)propanoate

: 159848-96-1
(3S,3S')-3--3-(4-methoxyphenyl)-1-propanol

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / 1M NaBH₃CN / methanol; acetic acid; tetrahydrofuran / 15 h / 0 - 14 °C

2: 94 percent / dioxane / 14 h / Ambient temperature

3: 97 percent / 2M LiBH₄ / diethyl ether; tetrahydrofuran / 13 h / Ambient temperature

With lithium borohydride; sodium cyanoborohydride; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; acetic acid;
DOI:10.1016/S0040-4020(01)85520-4