Technology Process of (3S,3S')-3--3-(4-methoxyphenyl)-1-propanol
There total 11 articles about (3S,3S')-3--3-(4-methoxyphenyl)-1-propanol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium borohydride;
In
tetrahydrofuran; diethyl ether;
for 13h;
Ambient temperature;
DOI:10.1016/S0040-4020(01)85520-4
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 4.75 percent / 1N NaOH / tetrahydrofuran / 4 h / Ambient temperature
2: 1.20 g / K2CO3 / dimethylformamide / 11 h / Ambient temperature
3: 94 percent / 10percent HCl / methanol / 1 h / Ambient temperature
4: 86 percent / 1M NaBH3CN / methanol; acetic acid; tetrahydrofuran / 15 h / 0 - 14 °C
5: 94 percent / dioxane / 14 h / Ambient temperature
6: 97 percent / 2M LiBH4 / diethyl ether; tetrahydrofuran / 13 h / Ambient temperature
With
hydrogenchloride; sodium hydroxide; lithium borohydride; sodium cyanoborohydride; potassium carbonate;
In
tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)85520-4
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / 1M NaBH3CN / methanol; acetic acid; tetrahydrofuran / 15 h / 0 - 14 °C
2: 94 percent / dioxane / 14 h / Ambient temperature
3: 97 percent / 2M LiBH4 / diethyl ether; tetrahydrofuran / 13 h / Ambient temperature
With
lithium borohydride; sodium cyanoborohydride;
In
tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; acetic acid;
DOI:10.1016/S0040-4020(01)85520-4
