1-butylcyclohexyl dibenzyl phosphate

Base Information

• Chemical Name: 1-butylcyclohexyl dibenzyl phosphate
• CAS No.: 1133062-80-2
• Molecular Formula: C₂₄H₃₃O₄P
• Molecular Weight: 416.497
• Mol file: 1133062-80-2.mol

Synonyms:1-butylcyclohexyl dibenzyl phosphate

Chemical Property of 1-butylcyclohexyl dibenzyl phosphate

Chemical Property:

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Technology Process of 1-butylcyclohexyl dibenzyl phosphate

There total 1 articles about 1-butylcyclohexyl dibenzyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1-butyl-cyclohexanol (5445-30-7) + dibenzyl N,N-diethylphosphoramidite (67746-43-4) → 1-butylcyclohexyl dibenzyl phosphate (1133062-80-2)

Guidance literature:

1-butyl-cyclohexanol; dibenzyl N,N-diethylphosphoramidite; With 1H-tetrazole; phenyl isocyanate; In dichloromethane; acetonitrile; at 20 ℃; for 16h; Inert atmosphere;

With dihydrogen peroxide; In dichloromethane; water; acetonitrile; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.tetlet.2008.12.065

upstream raw materials:

1-butyl-cyclohexanol

dibenzyl N,N-diethylphosphoramidite