ethyl 1-(2,3-dimethoxyphenyl)-4-oxocyclohex-2-enecarboxylate propylene acetal

Base Information

Chemical Name:ethyl 1-(2,3-dimethoxyphenyl)-4-oxocyclohex-2-enecarboxylate propylene acetal
CAS No.:115262-25-4
Molecular Formula:C₂₀H₂₆O₆
Molecular Weight:362.423
Hs Code.:

Synonyms:ethyl 1-(2,3-dimethoxyphenyl)-4-oxocyclohex-2-enecarboxylate propylene acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 1-(2,3-dimethoxyphenyl)-4-oxocyclohex-2-enecarboxylate propylene acetal

Chemical Property:

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Technology Process of ethyl 1-(2,3-dimethoxyphenyl)-4-oxocyclohex-2-enecarboxylate propylene acetal

There total 3 articles about ethyl 1-(2,3-dimethoxyphenyl)-4-oxocyclohex-2-enecarboxylate propylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 104331-23-9
ethyl 1-(2,3-dimethoxyphenyl)-4-oxocyclohex-2-enecarboxylate

: 504-63-2
trimethyleneglycol

: 115262-25-4
ethyl 1-(2,3-dimethoxyphenyl)-4-oxocyclohex-2-enecarboxylate propylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 20h; Heating;

Reference yield:

: 104331-18-2
ethyl 4-oxocyclohex-2-enecarboxylate

: 115262-25-4
ethyl 1-(2,3-dimethoxyphenyl)-4-oxocyclohex-2-enecarboxylate propylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridine; CHCl₃ / 1.) r.t.; 0.5 h; 2.) 55 deg C; 24 h

2: 88 percent / toluene-p-sulphonic acid / benzene / 20 h / Heating

With toluene-4-sulfonic acid; In pyridine; chloroform; benzene;

Reference yield:

: 104380-32-7
2,3-dimethoxyphenyl-lead triacetate

: 115262-25-4
ethyl 1-(2,3-dimethoxyphenyl)-4-oxocyclohex-2-enecarboxylate propylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridine; CHCl₃ / 1.) r.t.; 0.5 h; 2.) 55 deg C; 24 h

2: 88 percent / toluene-p-sulphonic acid / benzene / 20 h / Heating

With toluene-4-sulfonic acid; In pyridine; chloroform; benzene;