(5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)dimethanol

Base Information

Chemical Name:(5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)dimethanol
CAS No.:1355342-67-4
Molecular Formula:C₂₂H₂₉BO₅
Molecular Weight:384.28
Hs Code.:

Synonyms:(5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)dimethanol

Suppliers and Price of (5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)dimethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)dimethanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)dimethanol

There total 6 articles about (5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1355342-66-3
(((5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)bis(methylene))bis(oxy))bis(tertbutyldimethylsilane)

: 1355342-67-4
(5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)dimethanol

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 20 ℃; for 0.5h;
DOI:10.1002/asia.202100865

Reference yield:

: 633314-21-3
2,6-bis(((tert-butyldimethylsilyl)oxy)methyl)-4-methylphenol

: 1355342-67-4
(5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)dimethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 - 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / methanol / 0.5 h / 20 °C / Inert atmosphere

With potassium carbonate; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1039/c1ob06667f

Reference yield:

: 91-04-3
2,6-bis(hydroxymethyl)-4-methylphenol

: 1355342-67-4
(5-methyl-2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-1,3-phenylene)dimethanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C / Inert atmosphere

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid / methanol / 1 h / 20 °C / Inert atmosphere

With 1H-imidazole; potassium carbonate; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja303372u