Octanoic acid (R)-2-{benzyloxy-[(1S,2R,3R,4S,5S,6R)-3,5-bis-(bis-benzyloxy-phosphoryloxy)-2,4,6-tris-butyryloxy-cyclohexyloxy]-phosphoryloxy}-1-octanoyloxymethyl-ethyl ester

Base Information

Chemical Name:Octanoic acid (R)-2-{benzyloxy-[(1S,2R,3R,4S,5S,6R)-3,5-bis-(bis-benzyloxy-phosphoryloxy)-2,4,6-tris-butyryloxy-cyclohexyloxy]-phosphoryloxy}-1-octanoyloxymethyl-ethyl ester
CAS No.:377752-78-8
Molecular Formula:C₇₂H₉₇O₂₂P₃
Molecular Weight:1407.47
Hs Code.:

Octanoic acid (R)-2-{benzyloxy-[(1S,2R,3R,4S,5S,6R)-3,5-bis-(bis-benzyloxy-phosphoryloxy)-2,4,6-tris-butyryloxy-cyclohexyloxy]-phosphoryloxy}-1-octanoyloxymethyl-ethyl ester

Synonyms:Octanoic acid (R)-2-{benzyloxy-[(1S,2R,3R,4S,5S,6R)-3,5-bis-(bis-benzyloxy-phosphoryloxy)-2,4,6-tris-butyryloxy-cyclohexyloxy]-phosphoryloxy}-1-octanoyloxymethyl-ethyl ester

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Chemical Property of Octanoic acid (R)-2-{benzyloxy-[(1S,2R,3R,4S,5S,6R)-3,5-bis-(bis-benzyloxy-phosphoryloxy)-2,4,6-tris-butyryloxy-cyclohexyloxy]-phosphoryloxy}-1-octanoyloxymethyl-ethyl ester

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Technology Process of Octanoic acid (R)-2-{benzyloxy-[(1S,2R,3R,4S,5S,6R)-3,5-bis-(bis-benzyloxy-phosphoryloxy)-2,4,6-tris-butyryloxy-cyclohexyloxy]-phosphoryloxy}-1-octanoyloxymethyl-ethyl ester

There total 6 articles about Octanoic acid (R)-2-{benzyloxy-[(1S,2R,3R,4S,5S,6R)-3,5-bis-(bis-benzyloxy-phosphoryloxy)-2,4,6-tris-butyryloxy-cyclohexyloxy]-phosphoryloxy}-1-octanoyloxymethyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 163563-71-1
1,2-Di-O-octanoyl-sn-glycerol benzyl (N,N-diisopropylamino)phosphoramidite

: Butyric acid (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphoryloxy)-3,5-bis-butyryloxy-4-hydroxy-cyclohexyl ester

: 377752-78-8
Octanoic acid (R)-2-{benzyloxy-[(1S,2R,3R,4S,5S,6R)-3,5-bis-(bis-benzyloxy-phosphoryloxy)-2,4,6-tris-butyryloxy-cyclohexyloxy]-phosphoryloxy}-1-octanoyloxymethyl-ethyl ester

Guidance literature:: 1,2-Di-O-octanoyl-sn-glycerol benzyl (N,N-diisopropylamino)phosphoramidite; Butyric acid (1R,2S,3S,4R,5S,6R)-2,6-bis-(bis-benzyloxy-phosphoryloxy)-3,5-bis-butyryloxy-4-hydroxy-cyclohexyl ester; With 1H-tetrazole; In dichloromethane; at 25 ℃; for 72h;

With peracetic acid; at -30 - 25 ℃; for 1h;
DOI:10.1002/1521-3773(20010817)40:16<3004::AID-ANIE3004>3.0.CO;2-O

Reference yield:

: myo-inositol-1,3,5-O-orthoformate

: 377752-78-8
Octanoic acid (R)-2-{benzyloxy-[(1S,2R,3R,4S,5S,6R)-3,5-bis-(bis-benzyloxy-phosphoryloxy)-2,4,6-tris-butyryloxy-cyclohexyloxy]-phosphoryloxy}-1-octanoyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: DMAP / pyridine / 18 h / 25 °C

2.1: TFA / H₂O; methanol / 8 h / 25 °C

3.1: 50 percent / imidazole / dimethylformamide / 96 h / 25 °C

4.1: tetrazole / acetonitrile / 72 h / 25 °C

4.2: 32 percent CH₃CO₃H / 1 h / -30 - 25 °C

5.1: 98 percent / Et₃N*3HF / acetonitrile / 72 h / 25 °C

6.1: tetrazole / CH₂Cl₂ / 72 h / 25 °C

6.2: 32 percent CH₃CO₃H / 1 h / -30 - 25 °C

With 1H-imidazole; 1H-tetrazole; dmap; triethylamine tris(hydrogen fluoride); trifluoroacetic acid; In pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/1521-3773(20010817)40:16<3004::AID-ANIE3004>3.0.CO;2-O

Reference yield:

: butyric acid 8,9-bis-butyryloxy-2,4,10-trioxa-tricyclo[3.3.1.1^3,7]dec-6-yl ester

: 377752-78-8
Octanoic acid (R)-2-{benzyloxy-[(1S,2R,3R,4S,5S,6R)-3,5-bis-(bis-benzyloxy-phosphoryloxy)-2,4,6-tris-butyryloxy-cyclohexyloxy]-phosphoryloxy}-1-octanoyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: TFA / H₂O; methanol / 8 h / 25 °C

2.1: 50 percent / imidazole / dimethylformamide / 96 h / 25 °C

3.1: tetrazole / acetonitrile / 72 h / 25 °C

3.2: 32 percent CH₃CO₃H / 1 h / -30 - 25 °C

4.1: 98 percent / Et₃N*3HF / acetonitrile / 72 h / 25 °C

5.1: tetrazole / CH₂Cl₂ / 72 h / 25 °C

5.2: 32 percent CH₃CO₃H / 1 h / -30 - 25 °C

With 1H-imidazole; 1H-tetrazole; triethylamine tris(hydrogen fluoride); trifluoroacetic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/1521-3773(20010817)40:16<3004::AID-ANIE3004>3.0.CO;2-O