(S,Z)-4-(1-(4-methoxyphenyl)penta-1,4-dien-3-yl)phenyl 4-methylbenzenesulfonate

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Chemical Name:(S,Z)-4-(1-(4-methoxyphenyl)penta-1,4-dien-3-yl)phenyl 4-methylbenzenesulfonate
CAS No.:1547460-09-2
Molecular Formula:C₂₅H₂₄O₄S
Molecular Weight:420.529
Hs Code.:

Synonyms:(S,Z)-4-(1-(4-methoxyphenyl)penta-1,4-dien-3-yl)phenyl 4-methylbenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,Z)-4-(1-(4-methoxyphenyl)penta-1,4-dien-3-yl)phenyl 4-methylbenzenesulfonate

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Technology Process of (S,Z)-4-(1-(4-methoxyphenyl)penta-1,4-dien-3-yl)phenyl 4-methylbenzenesulfonate

There total 2 articles about (S,Z)-4-(1-(4-methoxyphenyl)penta-1,4-dien-3-yl)phenyl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: toluene-4-sulfonic acid 4-[3-(diethoxyphosphoryloxy)propenyl]phenyl ester

: 1430803-71-6
(Z)-2-(2-(4-methoxyphenyl)vinyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1547460-09-2
(S,Z)-4-(1-(4-methoxyphenyl)penta-1,4-dien-3-yl)phenyl 4-methylbenzenesulfonate

Guidance literature:: With C₃₇H₃₄N₂O₃S; sodium methylate; copper(l) chloride; In tetrahydrofuran; at 22 ℃; for 24h; enantioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/ja4126565

Reference yield:

: 637-69-4,24936-44-5
4-Methoxystyrene

: 1547460-09-2
(S,Z)-4-(1-(4-methoxyphenyl)penta-1,4-dien-3-yl)phenyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: N-{[(3-bromo-1-{3-bromo-2-[(tert-butyldimethylsilyl)oxy]-5,6,7,8-tetrahydronaphthalen-1-yl}-5,6,7,8-tetrahydronaphthalen-2-yl)oxy](2,5-dimethyl-1H-pyrrol-1-yl)(2-methyl-2-phenylpropylidene)molybdenumylidene}adamantan-1-amine / benzene / 4 h / 22 °C / 100 Torr

2: C₃₇H₃₄N₂O₃S; sodium methylate; copper(l) chloride / tetrahydrofuran / 24 h / 22 °C / Inert atmosphere; Sealed tube

With N-{[(3-bromo-1-{3-bromo-2-[(tert-butyldimethylsilyl)oxy]-5,6,7,8-tetrahydronaphthalen-1-yl}-5,6,7,8-tetrahydronaphthalen-2-yl)oxy](2,5-dimethyl-1H-pyrrol-1-yl)(2-methyl-2-phenylpropylidene)molybdenumylidene}adamantan-1-amine; C₃₇H₃₄N₂O₃S; sodium methylate; copper(l) chloride; In tetrahydrofuran; benzene;
DOI:10.1021/ja4126565

Reference yield: 79.0%

: 1547460-09-2
(S,Z)-4-(1-(4-methoxyphenyl)penta-1,4-dien-3-yl)phenyl 4-methylbenzenesulfonate

: 185020-38-6,96895-25-9
(+)-Nyasol

Guidance literature:: (S,Z)-4-(1-(4-methoxyphenyl)penta-1,4-dien-3-yl)phenyl 4-methylbenzenesulfonate; With potassium hydroxide; In ethanol; water; at 80 ℃; for 1h; Sealed tube; Inert atmosphere;

With hydrogenchloride; In ethanol; water; at 22 ℃; Inert atmosphere;

With methyl magnesium iodide; at 180 ℃; for 0.166667h; Sealed tube; Inert atmosphere;
DOI:10.1021/ja4126565