3-{[3-(ethoxycarbonyl)-5-methyl-1H-pyrazol-1-yl]methyl}benzenecarboxylic acid

Base Information

Chemical Name:3-{[3-(ethoxycarbonyl)-5-methyl-1H-pyrazol-1-yl]methyl}benzenecarboxylic acid
CAS No.:1225380-90-4
Molecular Formula:C₁₅H₁₆N₂O₄
Molecular Weight:288.303
Hs Code.:

Synonyms:3-{[3-(ethoxycarbonyl)-5-methyl-1H-pyrazol-1-yl]methyl}benzenecarboxylic acid

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Chemical Property of 3-{[3-(ethoxycarbonyl)-5-methyl-1H-pyrazol-1-yl]methyl}benzenecarboxylic acid

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Technology Process of 3-{[3-(ethoxycarbonyl)-5-methyl-1H-pyrazol-1-yl]methyl}benzenecarboxylic acid

There total 3 articles about 3-{[3-(ethoxycarbonyl)-5-methyl-1H-pyrazol-1-yl]methyl}benzenecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1225380-89-1
ethyl 1-[3-(tert-butoxycarbonyl)benzyl]-5-methyl-1H-pyrazole-3-carboxylate

: 1225380-90-4
3-{[3-(ethoxycarbonyl)-5-methyl-1H-pyrazol-1-yl]methyl}benzenecarboxylic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 6h;

Reference yield:

: 126062-63-3
1,1-dimethylethyl 3-bromomethylbenzoate

: 1225380-90-4
3-{[3-(ethoxycarbonyl)-5-methyl-1H-pyrazol-1-yl]methyl}benzenecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 16 h / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 6 h / 20 °C

With potassium tert-butylate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 4027-57-0
ethyl 5-methyl-1H-pyrazole-3-carboxylate

: 1225380-90-4
3-{[3-(ethoxycarbonyl)-5-methyl-1H-pyrazol-1-yl]methyl}benzenecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 16 h / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 6 h / 20 °C

With potassium tert-butylate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;