methyl threo-3-<(5-chloro-2-nitrophenyl)thio>-2-hydroxy-3-(4-methoxyphenyl)propionate

Base Information

Chemical Name:methyl threo-3-<(5-chloro-2-nitrophenyl)thio>-2-hydroxy-3-(4-methoxyphenyl)propionate
CAS No.:96087-08-0
Molecular Formula:C₁₇H₁₆ClNO₆S
Molecular Weight:397.836
Hs Code.:

Synonyms:methyl threo-3-<(5-chloro-2-nitrophenyl)thio>-2-hydroxy-3-(4-methoxyphenyl)propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl threo-3-<(5-chloro-2-nitrophenyl)thio>-2-hydroxy-3-(4-methoxyphenyl)propionate

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Technology Process of methyl threo-3-<(5-chloro-2-nitrophenyl)thio>-2-hydroxy-3-(4-methoxyphenyl)propionate

There total 1 articles about methyl threo-3-<(5-chloro-2-nitrophenyl)thio>-2-hydroxy-3-(4-methoxyphenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.5%

: 14371-79-0
2-nitro-5-chlorothiophenol

: 96125-49-4
methyl trans-3-(4-methoxyphenyl)glycidate

: 96087-08-0
methyl threo-3-<(5-chloro-2-nitrophenyl)thio>-2-hydroxy-3-(4-methoxyphenyl)propionate

Guidance literature:: With zinc diacetate; In toluene; for 3h; Ambient temperature;
DOI:10.1021/jm00106a032

Reference yield: 82.4%

: 96087-08-0
methyl threo-3-<(5-chloro-2-nitrophenyl)thio>-2-hydroxy-3-(4-methoxyphenyl)propionate

: 96125-21-2
3-(5-Chloro-2-nitro-phenylsulfanyl)-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid

Guidance literature:: With sodium hydroxide; In methanol; for 8h; Ambient temperature;
DOI:10.1021/jm00106a032

Reference yield:

: 96087-08-0
methyl threo-3-<(5-chloro-2-nitrophenyl)thio>-2-hydroxy-3-(4-methoxyphenyl)propionate

: 105487-94-3,96125-34-7
(2R,3R)-8-Chloro-5-[2-(ethyl-methyl-amino)-ethyl]-3-hydroxy-2-(4-methoxy-phenyl)-2,3-dihydro-5H-benzo[b][1,4]thiazepin-4-one

Guidance literature:: Multi-step reaction with 4 steps

1: 82.4 percent / 10percent NaOH / methanol / 8 h / Ambient temperature

2: 78.8 percent / H₂, AcOH / 10percent Pd/C / ethanol / 11 h / Ambient temperature

3: 80.3 percent / xylene / 24 h / Heating

4: 80 percent / aq. K₂CO₃ / acetone / 17 h / Heating

With sodium hydroxide; hydrogen; potassium carbonate; acetic acid; palladium on activated charcoal; In methanol; ethanol; acetone; xylene;
DOI:10.1021/jm00106a032