5'-deoxy-5'-<(4-methoxyphenyl)thio>-2',3'-O-isopropylideneadenosine

Base Information

Chemical Name:5'-deoxy-5'-<(4-methoxyphenyl)thio>-2',3'-O-isopropylideneadenosine
CAS No.:134609-09-9
Molecular Formula:C₂H₄O₂*C₂₀H₂₃N₅O₄S
Molecular Weight:489.552
Hs Code.:

Synonyms:5'-deoxy-5'-<(4-methoxyphenyl)thio>-2',3'-O-isopropylideneadenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-deoxy-5'-<(4-methoxyphenyl)thio>-2',3'-O-isopropylideneadenosine

Chemical Property:

Purity/Quality:

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Technology Process of 5'-deoxy-5'-<(4-methoxyphenyl)thio>-2',3'-O-isopropylideneadenosine

There total 1 articles about 5'-deoxy-5'-<(4-methoxyphenyl)thio>-2',3'-O-isopropylideneadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5335-87-5
4,4'-dimethoxyphenyl disulfide

: 362-75-4
2',3'-isopropylidene adenosine

: 64-19-7,77671-22-8
acetic acid

: 134609-09-9
5'-deoxy-5'-<(4-methoxyphenyl)thio>-2',3'-O-isopropylideneadenosine

Guidance literature:: With pyridine; tributylphosphine; Yield given. Multistep reaction; 1.) RT, 15 min;
DOI:10.1021/jm00106a028

Reference yield:

: 134609-09-9
5'-deoxy-5'-<(4-methoxyphenyl)thio>-2',3'-O-isopropylideneadenosine

: 119244-40-5,119244-41-6
5'-deoxy-5'-<(4-methoxyphenyl)sulfinyl>-2',3'-O-isopropylideneadenosine

: 9-[(3aR,4R,6S,6aS)-6-(4-Methoxy-benzenesulfonylmethyl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl]-9H-purin-6-ylamine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -40 - 20 ℃;
DOI:10.1021/jm00106a028

Reference yield:

: 134609-09-9
5'-deoxy-5'-<(4-methoxyphenyl)thio>-2',3'-O-isopropylideneadenosine

: 119244-42-7,119244-43-8
9-{(3aR,4R,6S,6aS)-6-[Fluoro-(4-methoxy-phenylsulfanyl)-methyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-9H-purin-6-ylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 20.1 g / 3-chloroperbenzoic acid / CH₂Cl₂ / -40 - 20 °C

2: (diethylamido)sulfur trifluoride / CH₂Cl₂ / 2.5 h / 45 °C

With (diethylamido)sulfur trifluoride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00106a028