Technology Process of 2-chloro-3-benzoylcyclohexene
There total 7 articles about 2-chloro-3-benzoylcyclohexene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1.1: hydrogenchloride; 3-chloro-benzenecarboperoxoic acid / water; N,N-dimethyl-formamide / 0.5 h / 25 °C
2.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / methanol / 3.5 h / 0 - 25 °C / Inert atmosphere
3.1: carbon tetrabromide / diethyl ether / 0.08 h / 0 °C
3.2: 3 h / 0 - 25 °C
4.1: ammonium chloride; tin / tetrahydrofuran / 24 h / 65 °C
5.1: Jones reagent / water; toluene / 0 °C
With
hydrogenchloride; tin; sodium tetrahydroborate; Jones reagent; carbon tetrabromide; cerium(III) chloride heptahydrate; ammonium chloride; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; diethyl ether; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/acs.orglett.8b00967
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / methanol / 3.5 h / 0 - 25 °C / Inert atmosphere
2.1: carbon tetrabromide / diethyl ether / 0.08 h / 0 °C
2.2: 3 h / 0 - 25 °C
3.1: ammonium chloride; tin / tetrahydrofuran / 24 h / 65 °C
4.1: Jones reagent / water; toluene / 0 °C
With
tin; sodium tetrahydroborate; Jones reagent; carbon tetrabromide; cerium(III) chloride heptahydrate; ammonium chloride;
In
tetrahydrofuran; methanol; diethyl ether; water; toluene;
DOI:10.1021/acs.orglett.8b00967