3-Chloro-4-phenylpyridine

Base Information

Chemical Name:3-Chloro-4-phenylpyridine
CAS No.:90732-01-7
Molecular Formula:C11H8ClN
Molecular Weight:189.644
Hs Code.:
DSSTox Substance ID:DTXSID90376584
Nikkaji Number:J2.773.421I
Wikidata:Q82165470
Mol file:90732-01-7.mol

Synonyms:3-chloro-4-phenylpyridine;90732-01-7;SCHEMBL3306203;DTXSID90376584;FVAFHXOWOYVPIV-UHFFFAOYSA-N;AKOS006293182;FT-0692115;1-(CHLOROACETYL)-4-(2-METHOXYPHENYL)PIPERAZINEHYDROCHLORIDE

Suppliers and Price of 3-Chloro-4-phenylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-CHLORO-4-PHENYLPYRIDINE 95.00%
5MG
$ 499.24

Alichem
3-Chloro-4-phenylpyridine
1g
$ 2866.05

Alichem
3-Chloro-4-phenylpyridine
500mg
$ 1617.60

Alichem
3-Chloro-4-phenylpyridine
250mg
$ 950.60

Total 9 raw suppliers

Chemical Property of 3-Chloro-4-phenylpyridine

Chemical Property:

Vapor Pressure:0.0109mmHg at 25°C
Refractive Index:1.588
Boiling Point:271.2 °C at 760 mmHg
PKA:3.12±0.18(Predicted)
Flash Point:143.9 °C
PSA：12.89000
Density:1.186 g/cm³
LogP:3.40200
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:189.0345270
Heavy Atom Count:13
Complexity:154

Purity/Quality:

98%Min ^*data from raw suppliers

3-CHLORO-4-PHENYLPYRIDINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(C=NC=C2)Cl

Technology Process of 3-Chloro-4-phenylpyridine

There total 11 articles about 3-Chloro-4-phenylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: (1R*,5R*)-5-azido-2-chloro-3-phenylcyclopent-2-enol

: 90732-01-7
3-chloro-4-phenylpyridine

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium carbonate; In 1,2-dichloro-ethane; at 80 ℃; Inert atmosphere;
DOI:10.1021/ja9049564

Reference yield: 80.0%

: 458532-90-6
3-chloro-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pyridine

: 90732-01-7
3-chloro-4-phenylpyridine

Guidance literature:: 3-chloro-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pyridine; phenylmagnesium halide; In tetrahydrofuran; at -78 - 20 ℃; for 2.25h; Inert atmosphere;

With trifluoroacetyl chloride; In tetrahydrofuran; at -78 - -40 ℃; for 18.5h; Further stages; Inert atmosphere;
DOI:10.1002/anie.201510027

Reference yield: 67.0%

: 88912-27-0
3-chloro-isonicotinic acid

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 90732-01-7
3-chloro-4-phenylpyridine

Guidance literature:: With diethyl bromomethylmalonate; [4,4′-di-tert-butyl-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C}iridium(III) hexafluorophosphate; caesium carbonate; at 55 ℃; for 22h; Irradiation;
DOI:10.1039/c6sc05533h