cesium 4-((E)-4-((E)-4-((1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl)carbamoyl)styryl)styryl)benzenesulfonate

Base Information

Chemical Name:cesium 4-((E)-4-((E)-4-((1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl)carbamoyl)styryl)styryl)benzenesulfonate
CAS No.:1402151-19-2
Molecular Formula:C₂₇H₂₆NO₇S*Cs
Molecular Weight:641.477
Hs Code.:

Synonyms:cesium 4-((E)-4-((E)-4-((1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl)carbamoyl)styryl)styryl)benzenesulfonate

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Chemical Property of cesium 4-((E)-4-((E)-4-((1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl)carbamoyl)styryl)styryl)benzenesulfonate

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Technology Process of cesium 4-((E)-4-((E)-4-((1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl)carbamoyl)styryl)styryl)benzenesulfonate

There total 6 articles about cesium 4-((E)-4-((E)-4-((1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl)carbamoyl)styryl)styryl)benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: cesium 4-((E)-4-((E)-4-sulfonatostyryl)styryl)benzoate

: 77-86-1
2-amino-2-hydroxymethyl-1,3-propanediol

: 1402151-19-2
cesium 4-((E)-4-((E)-4-((1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl)carbamoyl)styryl)styryl)benzenesulfonate

Guidance literature:: cesium 4-((E)-4-((E)-4-sulfonatostyryl)styryl)benzoate; With O-(6-chlorobenzo-triazol-1-yl)-N,N,N′,N′-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.5h;

2-amino-2-hydroxymethyl-1,3-propanediol; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h; Sonication;
DOI:10.1021/ja306162g

Reference yield:

: (E)-4-(4-(diethoxymethyl)styryl)benzonitrile

: 1402151-19-2
cesium 4-((E)-4-((E)-4-((1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl)carbamoyl)styryl)styryl)benzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / chloroform; water / 12 h / 20 °C

2.1: sodium t-butanolate / tetrahydrofuran / 1.58 h / Inert atmosphere

3.1: cesiumhydroxide monohydrate / water; 1,2-dimethoxyethane / 24 h / 20 - 120 °C / Autoclave; Sonication

4.1: O-(6-chlorobenzo-triazol-1-yl)-N,N,N′,N′-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

4.2: 24 h / 0 - 20 °C / Sonication

With cesiumhydroxide monohydrate; O-(6-chlorobenzo-triazol-1-yl)-N,N,N′,N′-tetramethyluronium hexafluorophosphate; acetic acid; sodium t-butanolate; In tetrahydrofuran; 1,2-dimethoxyethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/ja306162g

Reference yield:

: 1402151-17-0
ethyl 4-((E)-4-((E)-4-cyanostyryl)styryl)benzenesulfonate

: 1402151-19-2
cesium 4-((E)-4-((E)-4-((1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl)carbamoyl)styryl)styryl)benzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: cesiumhydroxide monohydrate / water; 1,2-dimethoxyethane / 24 h / 20 - 120 °C / Autoclave; Sonication

2.1: O-(6-chlorobenzo-triazol-1-yl)-N,N,N′,N′-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

2.2: 24 h / 0 - 20 °C / Sonication

With cesiumhydroxide monohydrate; O-(6-chlorobenzo-triazol-1-yl)-N,N,N′,N′-tetramethyluronium hexafluorophosphate; In 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja306162g