C₂₈H₃₅NO₂Si

Base Information

Chemical Name:C₂₈H₃₅NO₂Si
CAS No.:1395819-69-8
Molecular Formula:C₂₈H₃₅NO₂Si
Molecular Weight:445.677
Hs Code.:

C<sub>28</sub>H<sub>35</sub>NO<sub>2</sub>Si

Synonyms:C₂₈H₃₅NO₂Si

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Chemical Property of C₂₈H₃₅NO₂Si

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Technology Process of C₂₈H₃₅NO₂Si

There total 6 articles about C₂₈H₃₅NO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1395819-03-0
(3S)-3-tert-butyldiphenylsilyloxy-3,4,5,6-tetrahydropyridine N-oxide

: 6921-34-2
benzylmagnesium chloride

: 1395819-69-8
C₂₈H₃₅NO₂Si

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo3011914

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1395819-69-8
C₂₈H₃₅NO₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate; zinc(II) chloride; triethylamine / tetrahydrofuran / 4 h / 0 - 80 °C / Inert atmosphere

3.1: p-toluenesulfonyl chloride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: triethylamine; hydroxylamine hydrochloride / 4 h / Reflux; Inert atmosphere

5.1: manganese(IV) oxide / dichloromethane / 2 h / 0 °C / Inert atmosphere

6.1: tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With 1H-imidazole; manganese(IV) oxide; sodium tetrahydroborate; hydroxylamine hydrochloride; triethylamine; p-toluenesulfonyl chloride; zinc(II) chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo3011914

Reference yield:

: 1067244-41-0
(2S)-2-(tert-butyldiphenylsilyloxy)pentane-1,5-diol

: 1395819-69-8
C₂₈H₃₅NO₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: p-toluenesulfonyl chloride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: triethylamine; hydroxylamine hydrochloride / 4 h / Reflux; Inert atmosphere

3.1: manganese(IV) oxide / dichloromethane / 2 h / 0 °C / Inert atmosphere

4.1: tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With manganese(IV) oxide; hydroxylamine hydrochloride; triethylamine; p-toluenesulfonyl chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo3011914