S-(4-methoxyphenyl) 2-phenylethanethioate

Base Information

• Chemical Name: S-(4-methoxyphenyl) 2-phenylethanethioate
• CAS No.: 1236212-69-3
• Molecular Formula: C₁₅H₁₄O₂S
• Molecular Weight: 258.341
• Mol file: 1236212-69-3.mol

Synonyms:S-(4-methoxyphenyl) 2-phenylethanethioate

Chemical Property of S-(4-methoxyphenyl) 2-phenylethanethioate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of S-(4-methoxyphenyl) 2-phenylethanethioate

There total 2 articles about S-(4-methoxyphenyl) 2-phenylethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

tungsten hexacarbonyl (14040-11-0) + benzyl chloride (100-44-7) + 4-methoxy-phenyl-sulphonyl chloride (98-68-0) → S-(4-methoxyphenyl) 2-phenylethanethioate (1236212-69-3)

Guidance literature:

With water; palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In acetonitrile; at 100 ℃; for 24h; Inert atmosphere; Sealed tube;

DOI:10.1002/adsc.202100112

Reference yield: 78.0%

→ S-(4-methoxyphenyl) 2-phenylethanethioate (1236212-69-3)

Guidance literature:

With tungsten hexacarbonyl; palladium diacetate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In water; acetonitrile; at 100 ℃; for 24h; Schlenk technique;

Reference yield:

N-benzylidenephenylsulfonamide (13909-34-7) + S-(4-methoxyphenyl) 2-phenylethanethioate (1236212-69-3) → C28H25NO4S2 + C28H25NO4S2 + C28H25NO4S2

Guidance literature:

With 1-(3,5-bis(trifluoromethyl)phenyl)-3-((S)-((2S,4S,8R)-8-ethylquinuclidin-2-yl)(6-methoxyquinolin-4-yl)methyl)thiourea; In toluene; for 12h; diastereoselective reaction; Inert atmosphere;

DOI:10.1021/ol101152b

upstream raw materials:

tungsten hexacarbonyl

benzyl chloride

4-methoxy-phenyl-sulphonyl chloride