mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-pyridinecarboxaldimine)rhenium(III)

Base Information

Chemical Name:mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-pyridinecarboxaldimine)rhenium(III)
CAS No.:152978-57-9
Molecular Formula:C₃₁H₂₇Cl₃N₂OPRe
Molecular Weight:767.108
Hs Code.:

Synonyms:mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-pyridinecarboxaldimine)rhenium(III)

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Chemical Property of mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-pyridinecarboxaldimine)rhenium(III)

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Technology Process of mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-pyridinecarboxaldimine)rhenium(III)

There total 6 articles about mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-pyridinecarboxaldimine)rhenium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 7471-13-8
N-(pyrid-2-ylmethylene)-p-tolylamine

: [ReOCl₃(PPh₃)₂]

: 152978-57-9
mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-pyridinecarboxaldimine)rhenium(III)

Guidance literature:: In toluene; N2-atmosphere; stirring at 50°C for 10 min; filtration, evapn. (reduced pressure), dissoln. in CH2Cl2, chromy. (SiO2, C6H6, then C6H6/MeCN=20:1), crystn. on slow evapn.; elem. anal.;

Reference yield:

: 152978-59-1
ReCl₃(C₅H₄NCHNC₆H₄CH₃)(OP(C₆H₅)3)⁽¹⁺⁾

: ReCl₃(OP(C₆H₅)3)(C₅H₄NCONC₆H₄CH₃)*0.5C₆H₆

: 152978-57-9
mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-pyridinecarboxaldimine)rhenium(III)

Guidance literature:: With water; In acetonitrile; byproducts: H(1+); not isolated, detd. by UV/VIS spectroscopy and cyclic voltammetry; Kinetics;