mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-picolinamide)rhenium(IV)

Base Information

Chemical Name:mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-picolinamide)rhenium(IV)
CAS No.:153008-30-1
Molecular Formula:C₃₁H₂₆Cl₃N₂O₂PRe
Molecular Weight:782.099
Hs Code.:

Synonyms:mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-picolinamide)rhenium(IV)

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Chemical Property of mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-picolinamide)rhenium(IV)

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Technology Process of mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-picolinamide)rhenium(IV)

There total 3 articles about mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-picolinamide)rhenium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 152978-57-9
mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-pyridinecarboxaldimine)rhenium(III)

: 153008-30-1
mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-picolinamide)rhenium(IV)

Guidance literature:: With (NH₄)4[Ce(SO₄)4]*2H₂O; In dichloromethane; water; acetonitrile; addn. of aq. Ce-compd. to Re-complex (in CH2Cl2/MeCN=1:6), stirring for 2 h at room temp.; decantation, evapn. (reduced pressure), washing (water), drying (vac., over P2O5); elem. anal.;

Reference yield: 75.0%

: 152978-57-9
mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-pyridinecarboxaldimine)rhenium(III)

: 7722-84-1
dihydrogen peroxide

: 153008-30-1
mer-trichloro(triphenylphosphine oxide)(N-p-tolyl-2-picolinamide)rhenium(IV)

Guidance literature:: In acetonitrile; excess 30% H2O2, stirring for 1 h; evapn. (reduced pressure), washing (water), drying (vac., over P2O5), recrystn. (PhMe); elem. anal.;