Technology Process of C35H45N7O6
There total 12 articles about C35H45N7O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H33N5O7;
With
platinum/vanadium on charcoal; hydrogen;
In
ethanol; ethyl acetate;
at 38 ℃;
under 1810.07 Torr;
4-(N,N-dimethylamidino)benzoic acid hydrochloride;
With
N-(3-dimethylaminopropyl)-N-ethylcarbodiimide;
In
ethanol; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: boron tribromide / dichloromethane / 20 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 40 °C
3.1: lithium hydroxide / tetrahydrofuran; water / 1 h / 20 °C
4.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C
4.2: 0.5 h
5.1: palladium 10% on activated carbon; hydrogen / ethyl acetate
6.1: hydrogen; platinum/vanadium on charcoal / ethyl acetate; ethanol / 38 °C / 1810.07 Torr
With
platinum/vanadium on charcoal; palladium 10% on activated carbon; hydrogen; boron tribromide; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hydroxide / tetrahydrofuran; water / 1 h / 20 °C
2.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C
2.2: 0.5 h
3.1: palladium 10% on activated carbon; hydrogen / ethyl acetate
4.1: hydrogen; platinum/vanadium on charcoal / ethyl acetate; ethanol / 38 °C / 1810.07 Torr
With
platinum/vanadium on charcoal; palladium 10% on activated carbon; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; ethanol; water; ethyl acetate; N,N-dimethyl-formamide;