4-{3,5-Bis-[4-hydroxy-1,1-bis-(3-hydroxy-propyl)-butyl]-phenyl}-4-(3-hydroxy-propyl)-heptane-1,7-diol

Base Information

• Chemical Name: 4-{3,5-Bis-[4-hydroxy-1,1-bis-(3-hydroxy-propyl)-butyl]-phenyl}-4-(3-hydroxy-propyl)-heptane-1,7-diol
• CAS No.: 152339-16-7
• Molecular Formula: C₃₆H₆₆O₉
• Molecular Weight: 642.915

Synonyms:4-{3,5-Bis-[4-hydroxy-1,1-bis-(3-hydroxy-propyl)-butyl]-phenyl}-4-(3-hydroxy-propyl)-heptane-1,7-diol

Chemical Property of 4-{3,5-Bis-[4-hydroxy-1,1-bis-(3-hydroxy-propyl)-butyl]-phenyl}-4-(3-hydroxy-propyl)-heptane-1,7-diol

Chemical Property:

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Technology Process of 4-{3,5-Bis-[4-hydroxy-1,1-bis-(3-hydroxy-propyl)-butyl]-phenyl}-4-(3-hydroxy-propyl)-heptane-1,7-diol

There total 2 articles about 4-{3,5-Bis-[4-hydroxy-1,1-bis-(3-hydroxy-propyl)-butyl]-phenyl}-4-(3-hydroxy-propyl)-heptane-1,7-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1,3,5-Tris-(1,1-diallyl-but-3-enyl)-benzene (152339-15-6) → 4-{3,5-Bis-[4-hydroxy-1,1-bis-(3-hydroxy-propyl)-butyl]-phenyl}-4-(3-hydroxy-propyl)-heptane-1,7-diol (152339-16-7)

Guidance literature:

1,3,5-Tris-(1,1-diallyl-but-3-enyl)-benzene; With borane; isobutene; In tetrahydrofuran; at 20 ℃; for 12h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 50 ℃; for 12h;

DOI:10.1002/anie.200453870

Reference yield:

allyl bromide (106-95-6) → 4-{3,5-Bis-[4-hydroxy-1,1-bis-(3-hydroxy-propyl)-butyl]-phenyl}-4-(3-hydroxy-propyl)-heptane-1,7-diol (152339-16-7)

Guidance literature:

Multistep reaction.;

DOI:10.1039/B000370K

Reference yield: 95.0%

methanesulfonyl chloride (124-63-0) + 4-{3,5-Bis-[4-hydroxy-1,1-bis-(3-hydroxy-propyl)-butyl]-phenyl}-4-(3-hydroxy-propyl)-heptane-1,7-diol (152339-16-7) → methanesulfonic acid 4-{3,5-bis-[4-methanesulfonyloxy-1,1-bis-(3-methanesulfonyloxy-propyl)-butyl]-phenyl}-7-methanesulfonyloxy-4-(3-methanesulfonyloxy-propyl)-heptyl ester

Guidance literature:

With pyridine; at 0 ℃; for 5h;

DOI:10.1021/ja983868m

upstream raw materials:

1,3,5-Tris-(1,1-diallyl-but-3-enyl)-benzene

allyl bromide

Downstream raw materials:

1,3,5-tris-[4-iodo-1,1-bis-(3-iodo-propyl)-butyl]-benzene

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