C₁₄H₂₃BrO₂Si

Base Information

Chemical Name:C₁₄H₂₃BrO₂Si
CAS No.:1344113-44-5
Molecular Formula:C₁₄H₂₃BrO₂Si
Molecular Weight:331.325
Hs Code.:

C<sub>14</sub>H<sub>23</sub>BrO<sub>2</sub>Si

Synonyms:C₁₄H₂₃BrO₂Si

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Chemical Property of C₁₄H₂₃BrO₂Si

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Technology Process of C₁₄H₂₃BrO₂Si

There total 1 articles about C₁₄H₂₃BrO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 106-41-2
4-bromo-phenol

: 56310-18-0
di-tert-butylchlorosilane

: 1344113-44-5
C₁₄H₂₃BrO₂Si

Guidance literature:: 4-bromo-phenol; di-tert-butylchlorosilane; With 1H-imidazole; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

With N-Bromosuccinimide; In dichloromethane;

With water; sodium hydroxide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ja208572v

Reference yield:

: 1344113-44-5
C₁₄H₂₃BrO₂Si

: 17345-77-6
1-bromo-3,4-dihydroxybenzene

Guidance literature:: C₁₄H₂₃BrO₂Si; With palladium(II) trimethylacetate; [bis(acetoxy)iodo]benzene; In α,α,α-trifluorotoluene; at 120 ℃; Inert atmosphere;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

With water; In tetrahydrofuran;
DOI:10.1021/ja208572v

Reference yield:

: 1344113-44-5
C₁₄H₂₃BrO₂Si

: 66373-95-3
4-bromo-1,2-phenylene diacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium(II) trimethylacetate; [bis(acetoxy)iodo]benzene / α,α,α-trifluorotoluene / 120 °C / Inert atmosphere

1.2: 20 °C

2.1: pyridine

With pyridine; palladium(II) trimethylacetate; [bis(acetoxy)iodo]benzene; In α,α,α-trifluorotoluene;
DOI:10.1021/ja208572v