N-[2-(4-amino-3-[1,3]dioxan-2-ylmethyl-phenoxy)-ethyl]-3-anthracen-9-yl-N-methyl-propionamide

Base Information

Chemical Name:N-[2-(4-amino-3-[1,3]dioxan-2-ylmethyl-phenoxy)-ethyl]-3-anthracen-9-yl-N-methyl-propionamide
CAS No.:705961-55-3
Molecular Formula:C₃₁H₃₄N₂O₄
Molecular Weight:498.622
Hs Code.:

Synonyms:N-[2-(4-amino-3-[1,3]dioxan-2-ylmethyl-phenoxy)-ethyl]-3-anthracen-9-yl-N-methyl-propionamide

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Chemical Property of N-[2-(4-amino-3-[1,3]dioxan-2-ylmethyl-phenoxy)-ethyl]-3-anthracen-9-yl-N-methyl-propionamide

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Technology Process of N-[2-(4-amino-3-[1,3]dioxan-2-ylmethyl-phenoxy)-ethyl]-3-anthracen-9-yl-N-methyl-propionamide

There total 8 articles about N-[2-(4-amino-3-[1,3]dioxan-2-ylmethyl-phenoxy)-ethyl]-3-anthracen-9-yl-N-methyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 705961-52-0
3-anthracen-9-yl-N-[2-(3-[1,3]dioxan-2-ylmethyl-4-nitrophenoxy)-ethyl]-N-methyl-propionamide

: 705961-55-3
N-[2-(4-amino-3-[1,3]dioxan-2-ylmethyl-phenoxy)-ethyl]-3-anthracen-9-yl-N-methyl-propionamide

Guidance literature:: With sodium tetrahydroborate; copper acetylacetonate; In methanol; dichloromethane; isopropyl alcohol; for 0.5h; Heating;
DOI:10.1039/b400110a

Reference yield:

: 705961-44-0
3-[1,3]dioxan-2-ylmethyl-4-nitrophenol

: 705961-55-3
N-[2-(4-amino-3-[1,3]dioxan-2-ylmethyl-phenoxy)-ethyl]-3-anthracen-9-yl-N-methyl-propionamide

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / K₂CO₃ / dimethylformamide / 2 h / 90 °C

2: 98 percent / Amberlyst H-15 / tetrahydrofuran / 24 h / 20 °C

3: 89 percent / NaBH₄; iodine / tetrahydrofuran / 4 h / Heating

4: 93 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C

5: 89 percent / NaBH₄ / copper acetylacetonate / CH₂Cl₂; propan-2-ol; methanol / 0.5 h / Heating

With sodium tetrahydroborate; Amberlyst H-15; iodine; potassium carbonate; triethylamine; copper acetylacetonate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1039/b400110a

Reference yield:

: 2581-34-2,910311-23-8
3-methyl-4-nitrophenol

: 705961-55-3
N-[2-(4-amino-3-[1,3]dioxan-2-ylmethyl-phenoxy)-ethyl]-3-anthracen-9-yl-N-methyl-propionamide

Guidance literature:: Multi-step reaction with 9 steps

1.1: 91 percent / K₂CO₃ / dimethylformamide / 2 h / 90 °C

2.1: dimethylformamide / 24 h / Heating

2.2: 82 percent / aq. HCl / diethyl ether / 2 h / Heating

3.1: 93 percent / trifluoroacetic acid / 24 h / 20 °C

4.1: 92 percent / Amberlyst H-15 / CH₂Cl₂ / 16 h / 20 °C

5.1: 98 percent / K₂CO₃ / dimethylformamide / 2 h / 90 °C

6.1: 98 percent / Amberlyst H-15 / tetrahydrofuran / 24 h / 20 °C

7.1: 89 percent / NaBH₄; iodine / tetrahydrofuran / 4 h / Heating

8.1: 93 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C

9.1: 89 percent / NaBH₄ / copper acetylacetonate / CH₂Cl₂; propan-2-ol; methanol / 0.5 h / Heating

With sodium tetrahydroborate; Amberlyst H-15; iodine; potassium carbonate; triethylamine; trifluoroacetic acid; copper acetylacetonate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1039/b400110a