C₄₉H₉₄O₄Si₃

Base Information

Chemical Name:C₄₉H₉₄O₄Si₃
CAS No.:1297531-59-9
Molecular Formula:C₄₉H₉₄O₄Si₃
Molecular Weight:831.539
Hs Code.:

C<sub>49</sub>H<sub>94</sub>O<sub>4</sub>Si<sub>3</sub>

Synonyms:C₄₉H₉₄O₄Si₃

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Chemical Property of C₄₉H₉₄O₄Si₃

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Technology Process of C₄₉H₉₄O₄Si₃

There total 18 articles about C₄₉H₉₄O₄Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1297531-58-8
(1S,2S,6S,8S,Z)-1-(3,5-bis((triisopropylsilyl)oxy)phenyl)-10-cyclohexyl-2,6,8-trimethyl-1-((triethylsilyl)oxy)dec-9-en-5-yl pivalate

: 1297531-59-9
C₄₉H₉₄O₄Si₃

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 ℃;
DOI:10.1021/ol200834p

Reference yield:

: 765915-18-2
(2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentan-1-ol

: 1297531-59-9
C₄₉H₉₄O₄Si₃

Guidance literature:: Multi-step reaction with 9 steps

1: C₅H₅N*HO₃S; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C

2: chromium dichloride; nickel dichloride / tetrahydrofuran; dimethyl sulfoxide / 17 h / 20 °C / Inert atmosphere; Large scale reaction

3: dmap; triethylamine / dichloromethane / 32 h / 20 - 43 °C

4: 2-nitrobenzenesulfonyl hydrazide; triethylamine / dichloromethane / 96 h / 20 °C

5: palladium 10% on activated carbon; hydrogen / 36 h

6: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; acetonitrile / 20 °C / Darkness

7: lithium carbonate / acetonitrile; benzene / 60 h / Reflux

8: lithium hexamethyldisilazane / tetrahydrofuran; toluene / -78 - 0 °C / Inert atmosphere

9: diisobutylaluminium hydride / dichloromethane / -78 °C

With 1H-imidazole; chromium dichloride; dmap; palladium 10% on activated carbon; C₅H₅N*HO₃S; 2-nitrobenzenesulfonyl hydrazide; hydrogen; iodine; lithium carbonate; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; nickel dichloride; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; acetonitrile; benzene; 2: Nozaki-Hiyama-Kishi reaction;
DOI:10.1021/ol200834p

Reference yield:

: 1297531-39-5
(2S,4S)-5-((4-methoxybenzyl)oxy)-2,4-dimethylpentanal

: 1297531-59-9
C₄₉H₉₄O₄Si₃

Guidance literature:: Multi-step reaction with 8 steps

1: chromium dichloride; nickel dichloride / tetrahydrofuran; dimethyl sulfoxide / 17 h / 20 °C / Inert atmosphere; Large scale reaction

2: dmap; triethylamine / dichloromethane / 32 h / 20 - 43 °C

3: 2-nitrobenzenesulfonyl hydrazide; triethylamine / dichloromethane / 96 h / 20 °C

4: palladium 10% on activated carbon; hydrogen / 36 h

5: 1H-imidazole; iodine; triphenylphosphine / diethyl ether; acetonitrile / 20 °C / Darkness

6: lithium carbonate / acetonitrile; benzene / 60 h / Reflux

7: lithium hexamethyldisilazane / tetrahydrofuran; toluene / -78 - 0 °C / Inert atmosphere

8: diisobutylaluminium hydride / dichloromethane / -78 °C

With 1H-imidazole; chromium dichloride; dmap; palladium 10% on activated carbon; 2-nitrobenzenesulfonyl hydrazide; hydrogen; iodine; lithium carbonate; diisobutylaluminium hydride; triethylamine; triphenylphosphine; nickel dichloride; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; acetonitrile; benzene; 1: Nozaki-Hiyama-Kishi reaction;
DOI:10.1021/ol200834p