(2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(triphenylmethylimino)butanamide

Base Information

Chemical Name:(2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(triphenylmethylimino)butanamide
CAS No.:349148-63-6
Molecular Formula:C₃₂H₃₂N₂O₂
Molecular Weight:476.618
Hs Code.:

Synonyms:(2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(triphenylmethylimino)butanamide

Suppliers and Price of (2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(triphenylmethylimino)butanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(triphenylmethylimino)butanamide

Chemical Property:

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Technology Process of (2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(triphenylmethylimino)butanamide

There total 5 articles about (2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(triphenylmethylimino)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 349148-63-6
(2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(triphenylmethylimino)butanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: LDA / hexamethylphosphoric acid triamide; tetrahydrofuran / 2 h / -78 °C

1.2: hexamethylphosphoric acid triamide; tetrahydrofuran / 3 h / -78 °C

2.1: AlMe₃ / CH₂Cl₂; hexane / 1 h / 20 °C

3.1: PPh₃; DEAD / tetrahydrofuran / 3 h / 0 °C

4.1: H₂ / Pd/C / methanol / 2 h

5.1: Et₃N / CHCl₃ / 4 °C

With hydrogen; trimethylaluminum; triethylamine; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; chloroform; 3.1: Intramolecular Mitsunobu reaction;
DOI:10.1021/jo0014055

Reference yield:

: 349148-56-7
(3R,4R)-3-benzyl-4-(N-benzyloxycarbonylamino)-butyrolactone

: 349148-63-6
(2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(triphenylmethylimino)butanamide

Guidance literature:: Multi-step reaction with 4 steps

1: AlMe₃ / CH₂Cl₂; hexane / 1 h / 20 °C

2: PPh₃; DEAD / tetrahydrofuran / 3 h / 0 °C

3: H₂ / Pd/C / methanol / 2 h

4: Et₃N / CHCl₃ / 4 °C

With hydrogen; trimethylaluminum; triethylamine; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane; chloroform; 2: Intramolecular Mitsunobu reaction;
DOI:10.1021/jo0014055

Reference yield:

: 349148-60-3
(2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(benzyloxycarbonylimino)-butanamide

: 349148-63-6
(2R,3R)-N-methoxy-N-methyl-2-benzyl-3,4-(triphenylmethylimino)butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / methanol / 2 h

2: Et₃N / CHCl₃ / 4 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1021/jo0014055