but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide propylamide

Base Information

Chemical Name:but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide propylamide
CAS No.:675876-25-2
Molecular Formula:C₃₃H₃₃N₅O₇S
Molecular Weight:643.72
Hs Code.:

but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1<i>H</i>-pyrrol-2-yl]-methyl}-amide propylamide

Synonyms:but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide propylamide

Suppliers and Price of but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide propylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide propylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide propylamide

There total 4 articles about but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide propylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 36342-07-1
N-Propyl maleamic acid

: 88333-03-3,10340-91-7
Benzyl isocyanide

: Benzyl-[1-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-meth-(E)-ylidene]-amine

: 675876-25-2
but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide propylamide

Guidance literature:: In methanol; at 20 ℃; for 36h;
DOI:10.1021/jo030231z

Reference yield:

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 675876-25-2
but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide propylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / Et₃N; DMAP / CH₂Cl₂ / 15 h / 20 °C

2: TMOF / 20 °C

3: 70 percent / methanol / 36 h / 20 °C

With dmap; triethylamine; trimethyl orthoformate; In methanol; dichloromethane; 3: Ugi reaction;
DOI:10.1021/jo030231z

Reference yield:

: 54254-38-5
1-(2-nitrophenylsulfonyl)-1H-pyrrole-2-carboxaldehyde

: 675876-25-2
but-2-enedioic acid benzyl-{benzylcarbamoyl-[1-(2-nitro-benzenesulfonyl)-1H-pyrrol-2-yl]-methyl}-amide propylamide

Guidance literature:: Multi-step reaction with 2 steps

1: TMOF / 20 °C

2: 70 percent / methanol / 36 h / 20 °C

With trimethyl orthoformate; In methanol; 2: Ugi reaction;
DOI:10.1021/jo030231z