(E)-phenyl(5-(trifluoromethoxy)-2-((4-(trifluoromethoxy)phenyl)diazenyl)phenyl)methanone

Base Information

Chemical Name:(E)-phenyl(5-(trifluoromethoxy)-2-((4-(trifluoromethoxy)phenyl)diazenyl)phenyl)methanone
CAS No.:1581291-38-4
Molecular Formula:C₂₁H₁₂F₆N₂O₃
Molecular Weight:454.328
Hs Code.:

Synonyms:(E)-phenyl(5-(trifluoromethoxy)-2-((4-(trifluoromethoxy)phenyl)diazenyl)phenyl)methanone

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Chemical Property of (E)-phenyl(5-(trifluoromethoxy)-2-((4-(trifluoromethoxy)phenyl)diazenyl)phenyl)methanone

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Technology Process of (E)-phenyl(5-(trifluoromethoxy)-2-((4-(trifluoromethoxy)phenyl)diazenyl)phenyl)methanone

There total 3 articles about (E)-phenyl(5-(trifluoromethoxy)-2-((4-(trifluoromethoxy)phenyl)diazenyl)phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1246760-11-1
(E)-1,2-bis(4-(trifluoromethoxy)phenyl)diazene

: 108-88-3,15644-74-3,16713-13-6
toluene

: 1581291-38-4
(E)-phenyl(5-(trifluoromethoxy)-2-((4-(trifluoromethoxy)phenyl)diazenyl)phenyl)methanone

Guidance literature:: With tert-butyl methyl ether; palladium diacetate; In acetonitrile; at 80 ℃; for 24h; regioselective reaction;
DOI:10.1021/jo5000219

Reference yield: 44.0%

: 103-50-4
dibenzyl ether

: 1246760-11-1
(E)-1,2-bis(4-(trifluoromethoxy)phenyl)diazene

: 1581291-38-4
(E)-phenyl(5-(trifluoromethoxy)-2-((4-(trifluoromethoxy)phenyl)diazenyl)phenyl)methanone

Guidance literature:: With tert.-butylhydroperoxide; palladium diacetate; In acetic acid; 1,2-dichloro-ethane; at 60 ℃; for 12h; regiospecific reaction; Sealed tube;
DOI:10.1055/s-0035-1561380

Reference yield:

: 461-82-5
4-(trifluoromethoxy)aniline

: 1581291-38-4
(E)-phenyl(5-(trifluoromethoxy)-2-((4-(trifluoromethoxy)phenyl)diazenyl)phenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: copper(I) bromide; pyridine / toluene / 20 h / 60 °C / 760.05 Torr

2: tert-butyl methyl ether; palladium diacetate / acetonitrile / 24 h / 80 °C

With pyridine; tert-butyl methyl ether; palladium diacetate; copper(I) bromide; In toluene; acetonitrile;
DOI:10.1021/jo5000219