1,3-di[N¹-2-pyrimidinylsulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

Base Information

• Chemical Name: 1,3-di[N¹-2-pyrimidinylsulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane
• CAS No.: 935510-06-8
• Molecular Formula: C₂₀H₁₆Cl₆N₈O₄P₂S₂
• Molecular Weight: 771.196

Synonyms:1,3-di[N¹-2-pyrimidinylsulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

Chemical Property of 1,3-di[N¹-2-pyrimidinylsulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

Chemical Property:

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Technology Process of 1,3-di[N¹-2-pyrimidinylsulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

There total 1 articles about 1,3-di[N¹-2-pyrimidinylsulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.5%

sulfadiazine (68-35-9) → 1,3-di[N1-2-pyrimidinylsulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane (935510-06-8)

Guidance literature:

With phosphorus pentachloride; In benzene; at 15 ℃; for 0.5h;

DOI:10.1016/j.saa.2006.04.032

Reference yield: 60.0%

1,3-di[N1-2-pyrimidinylsulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane (935510-06-8) + glycine (56-40-6,18875-39-3,25718-94-9) → 1,3-di-[N1-2-pyrimidinylsulfanilamide]-2,4-di[aminoacetic acid]-2,4-dichlorocyclodiphosph[V]azane (935510-08-0)

Guidance literature:

In acetonitrile; for 3h; Heating;

DOI:10.1016/j.saa.2006.04.032

Reference yield: 35.8%

1,3-di[N1-2-pyrimidinylsulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane (935510-06-8) → 1,3-di[N1-2-pyrimidinylsulfanilamide]-2,4-disulfo-2,4-dichlorocyclodiphosph(V)azane (935510-07-9)

Guidance literature:

With sulfur; In acetonitrile; for 1h; Heating;

DOI:10.1016/j.saa.2006.04.032

upstream raw materials:

sulfadiazine

Downstream raw materials:

1,3-di[N¹-2-pyrimidinylsulfanilamide]-2,4-disulfo-2,4-dichlorocyclodiphosph(V)azane

1,3-di-[N¹-2-pyrimidinylsulfanilamide]-2,4-di[aminoacetic acid]-2,4-dichlorocyclodiphosph[V]azane

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