1-[2-(benzyloxy)-3-methoxyphenoxy]-3-[3-(benzyloxy)naphthalen-2-yloxy]propan-2-one

Base Information

Chemical Name:1-[2-(benzyloxy)-3-methoxyphenoxy]-3-[3-(benzyloxy)naphthalen-2-yloxy]propan-2-one
CAS No.:943638-18-4
Molecular Formula:C₃₄H₃₀O₆
Molecular Weight:534.609
Hs Code.:

Synonyms:1-[2-(benzyloxy)-3-methoxyphenoxy]-3-[3-(benzyloxy)naphthalen-2-yloxy]propan-2-one

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Chemical Property of 1-[2-(benzyloxy)-3-methoxyphenoxy]-3-[3-(benzyloxy)naphthalen-2-yloxy]propan-2-one

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Technology Process of 1-[2-(benzyloxy)-3-methoxyphenoxy]-3-[3-(benzyloxy)naphthalen-2-yloxy]propan-2-one

There total 9 articles about 1-[2-(benzyloxy)-3-methoxyphenoxy]-3-[3-(benzyloxy)naphthalen-2-yloxy]propan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 943638-43-5
1-[2-(benzyloxy)-3-methoxyphenoxy]-3-[3-(benzyloxy)naphthalen-2-yloxy]propan-2-ol

: 943638-18-4
1-[2-(benzyloxy)-3-methoxyphenoxy]-3-[3-(benzyloxy)naphthalen-2-yloxy]propan-2-one

Guidance literature:: With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1055/s-2007-966016

Reference yield:

: 100-39-0
benzyl bromide

: 943638-18-4
1-[2-(benzyloxy)-3-methoxyphenoxy]-3-[3-(benzyloxy)naphthalen-2-yloxy]propan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 33 percent / NaHCO₃ / dimethylformamide / 17 h / 100 °C

2: 96 percent / NaOH; BnEt₃NCl / tetrahydrofuran; H₂O / 17 h / 20 °C

3: 86 percent / K₂CO₃ / acetone / 38 h / 110 °C

4: 65 percent / NMO; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 1.5 h / 20 °C

With sodium hydroxide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; N-benzyl-N,N,N-triethylammonium chloride; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1055/s-2007-966016

Reference yield:

2-{[3-(benzyloxy)naphthalen-2-yloxy]methyl}oxirane: 943638-24-2
2-{[3-(benzyloxy)naphthalen-2-yloxy]methyl}oxirane

: 943638-18-4
1-[2-(benzyloxy)-3-methoxyphenoxy]-3-[3-(benzyloxy)naphthalen-2-yloxy]propan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / K₂CO₃ / acetone / 38 h / 110 °C

2: 65 percent / NMO; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 1.5 h / 20 °C

With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; potassium carbonate; In dichloromethane; acetone;
DOI:10.1055/s-2007-966016