(2-Diphenylacetylamino-acetylamino)-acetic acid 2,2-diphenyl-ethyl ester

Base Information

• Chemical Name: (2-Diphenylacetylamino-acetylamino)-acetic acid 2,2-diphenyl-ethyl ester
• CAS No.: 190127-06-1
• Molecular Formula: C₃₂H₃₀N₂O₄
• Molecular Weight: 506.601
• Mol file: 190127-06-1.mol

Synonyms:(2-Diphenylacetylamino-acetylamino)-acetic acid 2,2-diphenyl-ethyl ester

Chemical Property of (2-Diphenylacetylamino-acetylamino)-acetic acid 2,2-diphenyl-ethyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (2-Diphenylacetylamino-acetylamino)-acetic acid 2,2-diphenyl-ethyl ester

There total 2 articles about (2-Diphenylacetylamino-acetylamino)-acetic acid 2,2-diphenyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,2-diphenyl ethanol (1883-32-5) + (2-Diphenylacetylamino-acetylamino)-acetic acid ethyl ester (315199-22-5) → (2-Diphenylacetylamino-acetylamino)-acetic acid 2,2-diphenyl-ethyl ester (190127-06-1)

Guidance literature:

With 1,3-dichlorotetrabutyldistannoxane; In toluene; Heating;

DOI:10.1002/anie.199707281

Reference yield:

glycylglycine ethyl ester (627-74-7) → (2-Diphenylacetylamino-acetylamino)-acetic acid 2,2-diphenyl-ethyl ester (190127-06-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / Et₃N / tetrahydrofuran

2: 90 percent / (Bu₂SnCl)2O / toluene / Heating

With 1,3-dichlorotetrabutyldistannoxane; triethylamine; In tetrahydrofuran; toluene;

DOI:10.1002/anie.199707281

Reference yield: 62.0%

p-xylylidenediamine (539-48-0) + benzene-1,3-dicarbonyl dichloride (99-63-8) + (2-Diphenylacetylamino-acetylamino)-acetic acid 2,2-diphenyl-ethyl ester (190127-06-1) → C32H30N2O4*C32H28N4O4

Guidance literature:

With triethylamine; In chloroform;

DOI:10.1002/chem.200305662

upstream raw materials:

2,2-diphenyl ethanol

(2-Diphenylacetylamino-acetylamino)-acetic acid ethyl ester

glycylglycine ethyl ester