17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanohydroxamic acid

Base Information

Chemical Name:17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanohydroxamic acid
CAS No.:868836-25-3
Molecular Formula:C₄₈H₆₆N₄O₇S₂
Molecular Weight:875.207
Hs Code.:

17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanohydroxamic acid

Synonyms:17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanohydroxamic acid

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Chemical Property of 17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanohydroxamic acid

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Technology Process of 17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanohydroxamic acid

There total 6 articles about 17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.8%

: 868836-21-9
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanoic acid

: 868836-25-3
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanohydroxamic acid

Guidance literature:: 17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanoic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.333333h;

With hydroxylamine; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;
DOI:10.1021/jm0505009

Reference yield: 75.8%

: 868836-25-3
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanohydroxamic acid

Guidance literature:

Reference yield:

: C₃₃H₄₁N₃O₆S₂

: 868836-25-3
17-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[3,3-(diphenyl)propyl]}amino-13-[N-2,4,6-(trimethyl)benzenesulfonyl]-8-oxo-7,11-diazaheptadecanohydroxamic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / dimethylformamide / 0.5 h / 0 °C

1.2: 60.3 percent / dimethylformamide / 12 h

2.1: 78.5 percent / hydrazine / methanol / 12 h / Heating

3.1: 75.1 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

4.1: 72.8 percent / aq. LiOH / tetrahydrofuran / 0 - 20 °C

5.1: ethyl chloroformate; triethylamine / tetrahydrofuran / 0.33 h / 0 °C

5.2: 75.8 percent / hydroxylamine / methanol; tetrahydrofuran / 0.5 h / 20 °C

With lithium hydroxide; chloroformic acid ethyl ester; sodium hydride; triethylamine; hydrazine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0505009