(E)-2-(2-(3-(3,4-dihydroxyphenyl)acrylamido)ethoxy)ethyl 4-hydroxy-3,5-dimethoxybenzoate

Base Information

Chemical Name:(E)-2-(2-(3-(3,4-dihydroxyphenyl)acrylamido)ethoxy)ethyl 4-hydroxy-3,5-dimethoxybenzoate
CAS No.:1254929-50-4
Molecular Formula:C₂₂H₂₅NO₉
Molecular Weight:447.442
Hs Code.:

Synonyms:(E)-2-(2-(3-(3,4-dihydroxyphenyl)acrylamido)ethoxy)ethyl 4-hydroxy-3,5-dimethoxybenzoate

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Chemical Property of (E)-2-(2-(3-(3,4-dihydroxyphenyl)acrylamido)ethoxy)ethyl 4-hydroxy-3,5-dimethoxybenzoate

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Technology Process of (E)-2-(2-(3-(3,4-dihydroxyphenyl)acrylamido)ethoxy)ethyl 4-hydroxy-3,5-dimethoxybenzoate

There total 4 articles about (E)-2-(2-(3-(3,4-dihydroxyphenyl)acrylamido)ethoxy)ethyl 4-hydroxy-3,5-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1254929-49-1
(E)-4-(3-(2-(2-(4-acetoxy-3,5-dimethoxybenzoyloxy)ethoxy)ethylamino)-3-oxoprop-1-enyl)-1,2-phenylene diacetate

: 1254929-50-4
(E)-2-(2-(3-(3,4-dihydroxyphenyl)acrylamido)ethoxy)ethyl 4-hydroxy-3,5-dimethoxybenzoate

Guidance literature:: With hydrazine hydrate; In methanol; at 20 ℃; for 0.5h;
DOI:10.5012/bkcs.2011.32.8.2593

Reference yield:

: 88623-81-8
3,4-diacetoxycinnamic acid

: 1254929-50-4
(E)-2-(2-(3-(3,4-dihydroxyphenyl)acrylamido)ethoxy)ethyl 4-hydroxy-3,5-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

2.1: dichloromethane

3.1: dmap / dichloromethane / 0.25 h

3.2: 3 h / Cooling with ice

4.1: hydrazine hydrate / methanol / 0.5 h / 20 °C

With dmap; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.5012/bkcs.2011.32.8.2593

Reference yield:

: 220957-78-8
3,4-di-O-acetylcaffeic acid N-hydroxysuccinimidyl ester

: 1254929-50-4
(E)-2-(2-(3-(3,4-dihydroxyphenyl)acrylamido)ethoxy)ethyl 4-hydroxy-3,5-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane

2.1: dmap / dichloromethane / 0.25 h

2.2: 3 h / Cooling with ice

3.1: hydrazine hydrate / methanol / 0.5 h / 20 °C

With dmap; hydrazine hydrate; In methanol; dichloromethane;
DOI:10.5012/bkcs.2011.32.8.2593