(E)-4-(3-(2-(2-(4-acetoxy-3,5-dimethoxybenzoyloxy)ethoxy)ethylamino)-3-oxoprop-1-enyl)-1,2-phenylene diacetate

Base Information

Chemical Name:(E)-4-(3-(2-(2-(4-acetoxy-3,5-dimethoxybenzoyloxy)ethoxy)ethylamino)-3-oxoprop-1-enyl)-1,2-phenylene diacetate
CAS No.:1254929-49-1
Molecular Formula:C₂₈H₃₁NO₁₂
Molecular Weight:573.554
Hs Code.:

Synonyms:(E)-4-(3-(2-(2-(4-acetoxy-3,5-dimethoxybenzoyloxy)ethoxy)ethylamino)-3-oxoprop-1-enyl)-1,2-phenylene diacetate

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Chemical Property of (E)-4-(3-(2-(2-(4-acetoxy-3,5-dimethoxybenzoyloxy)ethoxy)ethylamino)-3-oxoprop-1-enyl)-1,2-phenylene diacetate

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Technology Process of (E)-4-(3-(2-(2-(4-acetoxy-3,5-dimethoxybenzoyloxy)ethoxy)ethylamino)-3-oxoprop-1-enyl)-1,2-phenylene diacetate

There total 3 articles about (E)-4-(3-(2-(2-(4-acetoxy-3,5-dimethoxybenzoyloxy)ethoxy)ethylamino)-3-oxoprop-1-enyl)-1,2-phenylene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1254929-61-7
C₁₇H₂₁NO₇

: 39657-47-1
O-acetylsyringic acid chloride

: 1254929-49-1
(E)-4-(3-(2-(2-(4-acetoxy-3,5-dimethoxybenzoyloxy)ethoxy)ethylamino)-3-oxoprop-1-enyl)-1,2-phenylene diacetate

Guidance literature:: C₁₇H₂₁NO₇; With dmap; In dichloromethane; for 0.25h;

O-acetylsyringic acid chloride; In dichloromethane; for 3h; Cooling with ice;
DOI:10.5012/bkcs.2011.32.8.2593

Reference yield:

: 88623-81-8
3,4-diacetoxycinnamic acid

: 1254929-49-1
(E)-4-(3-(2-(2-(4-acetoxy-3,5-dimethoxybenzoyloxy)ethoxy)ethylamino)-3-oxoprop-1-enyl)-1,2-phenylene diacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane

2.1: dichloromethane

3.1: dmap / dichloromethane / 0.25 h

3.2: 3 h / Cooling with ice

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.5012/bkcs.2011.32.8.2593

Reference yield:

: 220957-78-8
3,4-di-O-acetylcaffeic acid N-hydroxysuccinimidyl ester

: 1254929-49-1
(E)-4-(3-(2-(2-(4-acetoxy-3,5-dimethoxybenzoyloxy)ethoxy)ethylamino)-3-oxoprop-1-enyl)-1,2-phenylene diacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane

2.1: dmap / dichloromethane / 0.25 h

2.2: 3 h / Cooling with ice

With dmap; In dichloromethane;
DOI:10.5012/bkcs.2011.32.8.2593