Technology Process of (S)-4,5-ISOPROPYLIDENE HEXANONITRILE
There total 5 articles about (S)-4,5-ISOPROPYLIDENE HEXANONITRILE which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: CBr4, triphenylphosphine / CH2Cl2 / 0.33 h / Ambient temperature; 1.) 0 deg C
2: hexamethylphosphoric acid triamide / 5 h
With
carbon tetrabromide; triphenylphosphine;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: LiAlH4 / diethyl ether / 1 h / Heating
2: CBr4, triphenylphosphine / CH2Cl2 / 0.33 h / Ambient temperature; 1.) 0 deg C
3: hexamethylphosphoric acid triamide / 5 h
With
lithium aluminium tetrahydride; carbon tetrabromide; triphenylphosphine;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: p-toluenesulphonic acid / 4 h / Heating
2: LiAlH4 / diethyl ether / 1 h / Heating
3: CBr4, triphenylphosphine / CH2Cl2 / 0.33 h / Ambient temperature; 1.) 0 deg C
4: hexamethylphosphoric acid triamide / 5 h
With
lithium aluminium tetrahydride; carbon tetrabromide; toluene-4-sulfonic acid; triphenylphosphine;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
