C₆H₅CONHCH⁽²⁾HCOOCH₃

Base Information

• Chemical Name: C₆H₅CONHCH⁽²⁾HCOOCH₃
• CAS No.: 119813-59-1
• Molecular Formula: C₁₀H₁₁NO₃
• Molecular Weight: 194.194
• Mol file: 119813-59-1.mol

Synonyms:C₆H₅CONHCH⁽²⁾HCOOCH₃

Chemical Property of C₆H₅CONHCH⁽²⁾HCOOCH₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of C₆H₅CONHCH⁽²⁾HCOOCH₃

There total 3 articles about C₆H₅CONHCH⁽²⁾HCOOCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

N-benzoyl-2-bromoglycine methyl ester (101649-82-5) → C6H5CONHCH(2)HCOOCH3 (119813-59-1)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tributyltin deuteride; In toluene; at 85 ℃; for 1.5h;

DOI:10.1039/c39880001030

Reference yield: 67.0%

tributyltin deuteride (6180-99-0) → C6H5CONHCH(2)HCOOCH3 (119813-59-1)

Guidance literature:

With catalyst: azoisobutyronitrile; In toluene; 2 equiv. stannane, 85°C, 1.5 h;

DOI:10.1039/c39880001030

Reference yield:

methyl hippurate (1205-08-9) → C6H5CONHCH(2)HCOOCH3 (119813-59-1)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; water-d2; lithium diisopropyl amide; Mechanism; Product distribution; multistep reaction; different reaction conditions, other deuteration reagents, effect of different amounts of LDA;

DOI:10.1016/S0040-4020(01)88213-2

upstream raw materials:

methyl hippurate

N-benzoyl-2-bromoglycine methyl ester

tributyltin deuteride