Technology Process of C62H48N2O4
There total 13 articles about C62H48N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
at 30 ℃;
for 12h;
Inert atmosphere;
DOI:10.1016/j.tet.2010.11.012
- Guidance literature:
-
With
piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
at 20 - 30 ℃;
for 12.0833h;
Inert atmosphere;
DOI:10.1021/ol8009623
- Guidance literature:
-
Multi-step reaction with 4 steps
1: methanol; potassium carbonate / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 12 h / 40 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 20 °C / Inert atmosphere
4: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / 12 h / 30 °C / Inert atmosphere
With
piperidine; methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine;
In
tetrahydrofuran;
2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1016/j.tet.2010.11.012