dimethyl phenylene-1,4-bis(methyl)phosphinate

Base Information

Chemical Name:dimethyl phenylene-1,4-bis(methyl)phosphinate
CAS No.:10580-44-6
Molecular Formula:C₁₀H₁₆O₄P₂
Molecular Weight:262.182
Hs Code.:

Synonyms:dimethyl phenylene-1,4-bis(methyl)phosphinate

Suppliers and Price of dimethyl phenylene-1,4-bis(methyl)phosphinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 22 raw suppliers

Chemical Property of dimethyl phenylene-1,4-bis(methyl)phosphinate

Chemical Property:

Purity/Quality:: 99% ,98%,Electron Grade , ^*data from raw suppliers

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Technology Process of dimethyl phenylene-1,4-bis(methyl)phosphinate

There total 3 articles about dimethyl phenylene-1,4-bis(methyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 106-37-6
1.4-dibromobenzene

: 16391-06-3
methyl hypophosphorous acid methyl ester

: 10580-44-6
dimethyl phenylene-1,4-bis(methyl)phosphinate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In 1,4-dioxane; at 60 ℃; for 96h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.201800884

Reference yield:

: 1179-06-2
1,4-Bis(diphenylphosphino)benzene

: 10580-44-6
dimethyl phenylene-1,4-bis(methyl)phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: (i) PCl₃, (ii) /BRN= 1098229/, Et₃N, Et₂O, THF

2: benzene

In benzene;
DOI:10.1021/jo01282a020