Methanesulfonic acid 3-[{(1R,2R)-2-[methyl-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-propyl ester

Base Information

Chemical Name:Methanesulfonic acid 3-[{(1R,2R)-2-[methyl-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-propyl ester
CAS No.:852043-23-3
Molecular Formula:C₂₅H₃₆N₂O₇S₃
Molecular Weight:572.768
Hs Code.:

Synonyms:Methanesulfonic acid 3-[{(1R,2R)-2-[methyl-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-propyl ester

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Chemical Property of Methanesulfonic acid 3-[{(1R,2R)-2-[methyl-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-propyl ester

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Technology Process of Methanesulfonic acid 3-[{(1R,2R)-2-[methyl-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-propyl ester

There total 4 articles about Methanesulfonic acid 3-[{(1R,2R)-2-[methyl-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124-63-0
methanesulfonyl chloride

: 852043-22-2
C₂₄H₃₄N₂O₅S₂

: 852043-23-3
Methanesulfonic acid 3-[{(1R,2R)-2-[methyl-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-propyl ester

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2005.02.141

Reference yield:

: 852043-13-1
C₄₂H₄₆N₂O₅S₂

: 852043-23-3
Methanesulfonic acid 3-[{(1R,2R)-2-[methyl-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / cesium carbonate / toluene / 1 h / 110 °C

2: 90 percent / trifluoroacetic acid / methanol; CH₂Cl₂ / 12 h / 20 °C

3: 100 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With caesium carbonate; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; toluene;
DOI:10.1021/jo0619837

Reference yield:

: 852043-21-1
C₄₃H₄₈N₂O₅S₂

: 852043-23-3
Methanesulfonic acid 3-[{(1R,2R)-2-[methyl-(toluene-4-sulfonyl)-amino]-cyclohexyl}-(toluene-4-sulfonyl)-amino]-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / trifluoroacetic acid / methanol; CH₂Cl₂ / 12 h / 20 °C

2: 100 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With triethylamine; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1021/jo0619837