toluene-4-sulfonic acid 4-[(naphthalene-1-sulfonylamino)-methyl]-cyclohexylmethyl ester

Base Information

Chemical Name:toluene-4-sulfonic acid 4-[(naphthalene-1-sulfonylamino)-methyl]-cyclohexylmethyl ester
CAS No.:192323-20-9
Molecular Formula:C₂₅H₂₉NO₅S₂
Molecular Weight:487.641
Hs Code.:

Synonyms:toluene-4-sulfonic acid 4-[(naphthalene-1-sulfonylamino)-methyl]-cyclohexylmethyl ester

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Chemical Property of toluene-4-sulfonic acid 4-[(naphthalene-1-sulfonylamino)-methyl]-cyclohexylmethyl ester

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Technology Process of toluene-4-sulfonic acid 4-[(naphthalene-1-sulfonylamino)-methyl]-cyclohexylmethyl ester

There total 3 articles about toluene-4-sulfonic acid 4-[(naphthalene-1-sulfonylamino)-methyl]-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85-46-1
1-Naphthalenesulfonyl chloride

: 192323-20-9
toluene-4-sulfonic acid 4-[(naphthalene-1-sulfonylamino)-methyl]-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / 1N aq. NaOH / 20 °C

2: LiAlH₄ / tetrahydrofuran / Heating

3: 90 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

With dmap; sodium hydroxide; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane; 1: sulfonylation / 2: Reduction / 3: Tosylation;
DOI:10.1016/S0960-894X(00)00177-3

Reference yield:

: 1197-18-8
trans-4-aminomethyl-cyclohexyl-carboxylic acid

: 192323-20-9
toluene-4-sulfonic acid 4-[(naphthalene-1-sulfonylamino)-methyl]-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / 1N aq. NaOH / 20 °C

2: LiAlH₄ / tetrahydrofuran / Heating

3: 90 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

With dmap; sodium hydroxide; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane; 1: sulfonylation / 2: Reduction / 3: Tosylation;
DOI:10.1016/S0960-894X(00)00177-3

Reference yield:

: 192322-99-9
4-[(naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarboxylic acid

: 192323-20-9
toluene-4-sulfonic acid 4-[(naphthalene-1-sulfonylamino)-methyl]-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / Heating

2: 90 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

With dmap; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane; 1: Reduction / 2: Tosylation;
DOI:10.1016/S0960-894X(00)00177-3