N²-<4,4',4''-tris(benzoyloxy)trityl>-N¹,N²-bis(benzoyloxy)ethylenedeoxyguanosine

Base Information

• Chemical Name: N²-<4,4',4''-tris(benzoyloxy)trityl>-N¹,N²-bis(benzoyloxy)ethylenedeoxyguanosine
• CAS No.: 106180-03-4
• Molecular Formula: C₇₄H₆₅N₅O₁₆
• Molecular Weight: 1280.35

Synonyms:N²-<4,4',4''-tris(benzoyloxy)trityl>-N¹,N²-bis(benzoyloxy)ethylenedeoxyguanosine

Chemical Property of N²-<4,4',4''-tris(benzoyloxy)trityl>-N¹,N²-bis(benzoyloxy)ethylenedeoxyguanosine

Chemical Property:

Purity/Quality:

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Technology Process of N²-<4,4',4''-tris(benzoyloxy)trityl>-N¹,N²-bis(benzoyloxy)ethylenedeoxyguanosine

There total 2 articles about N²-<4,4',4''-tris(benzoyloxy)trityl>-N¹,N²-bis(benzoyloxy)ethylenedeoxyguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C58H55N5O12 → N2-<4,4',4''-tris(benzoyloxy)trityl>-N1,N2-bis(benzoyloxy)ethylenedeoxyguanosine (106180-03-4)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: triethylamine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 17 h / Ambient temperature

With dmap; triethylamine; In pyridine; dichloromethane;

DOI:10.1246/bcsj.59.1781

Reference yield:

benzoic acid anhydride (93-97-0) + C60H57N5O14 (106180-02-3) → N2-<4,4',4''-tris(benzoyloxy)trityl>-N1,N2-bis(benzoyloxy)ethylenedeoxyguanosine (106180-03-4)

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 17h; Ambient temperature;

DOI:10.1246/bcsj.59.1781

Reference yield: 55.0%

N2-<4,4',4''-tris(benzoyloxy)trityl>-N1,N2-bis(benzoyloxy)ethylenedeoxyguanosine (106180-03-4) → C66H49N5O14 (106179-96-8)

Guidance literature:

With zinc dibromide; In dichloromethane; isopropyl alcohol; for 1h;

DOI:10.1246/bcsj.59.1781

upstream raw materials:

benzoic acid anhydride

C₆₀H₅₇N₅O₁₄

Downstream raw materials:

C₆₆H₄₉N₅O₁₄

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