isosorbide di(methyl carbonate)

Base Information

• Chemical Name: isosorbide di(methyl carbonate)
• CAS No.: 1235553-24-8
• Molecular Formula: C₁₀H₁₄O₈
• Molecular Weight: 262.216

Synonyms:isosorbide di(methyl carbonate)

Chemical Property of isosorbide di(methyl carbonate)

Chemical Property:

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Technology Process of isosorbide di(methyl carbonate)

There total 3 articles about isosorbide di(methyl carbonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

carbonic acid dimethyl ester (616-38-6) + Isosorbide (652-67-5) → C9H14O6 (1235553-26-0) + C9H14O6 (1235553-25-9) + isosorbide di(methyl carbonate) (1235553-24-8) + isosorbide dimethyl ether (5306-85-4)

Guidance literature:

With sodium methylate; at 90 ℃; for 20h; under 750.075 Torr; Inert atmosphere;

DOI:10.1002/cssc.201000011

Reference yield: 8.0%

carbonic acid dimethyl ester (616-38-6) + Isosorbide (652-67-5) → C9H14O6 (1235553-26-0) + C9H14O6 (1235553-25-9) + isosorbide di(methyl carbonate) (1235553-24-8) + (1R,4S,5R,8R)-8-methoxy-2,6-dioxabicyclo[3.3.0]octanol (162426-86-0) + (1R,4S,5R,8R)-4-methoxy-2,6-dioxabicyclo[3.3.0]octanol (6941-54-4) + isosorbide dimethyl ether (5306-85-4)

Guidance literature:

With sodium methylate; at 90 ℃; for 20h; under 750.075 Torr; Inert atmosphere;

DOI:10.1002/cssc.201000011

Reference yield:

D-sorbitol (50-70-4) + carbonic acid dimethyl ester (616-38-6) → isosorbide di(methyl carbonate) (1235553-24-8) + (1R,4S,5R,8R)-8-methoxy-2,6-dioxabicyclo[3.3.0]octanol (162426-86-0) + (1R,4S,5R,8R)-4-methoxy-2,6-dioxabicyclo[3.3.0]octanol (6941-54-4) + isosorbide dimethyl ether (5306-85-4)

Guidance literature:

With 1-Methylpyrrolidine; at 200 ℃; for 20h; under 15001.5 Torr; chemoselective reaction; Autoclave;

DOI:10.1039/d1cy00465d

upstream raw materials:

carbonic acid dimethyl ester

Isosorbide

D-sorbitol

Downstream raw materials:

isosorbide dimethyl ether

(1R,4S,5R,8R)-8-methoxy-2,6-dioxabicyclo[3.3.0]octanol

(1R,4S,5R,8R)-4-methoxy-2,6-dioxabicyclo[3.3.0]octanol

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