N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>dithiocarbamidsaeure

Base Information

• Chemical Name: N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>dithiocarbamidsaeure
• CAS No.: 96924-45-7
• Molecular Formula: C₁₆H₂₄N₂OS₂
• Molecular Weight: 324.511
• Mol file: 96924-45-7.mol

Synonyms:N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>dithiocarbamidsaeure

Chemical Property of N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>dithiocarbamidsaeure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>dithiocarbamidsaeure

There total 1 articles about N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>dithiocarbamidsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

carbon disulfide (75-15-0,12122-00-8) + N-<3-<3-(1-piperidinylmethyl)phenoxy>propyl>amine (73278-98-5) → N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>dithiocarbamidsaeure (96924-45-7)

Guidance literature:

In ethanol; for 1h;

DOI:10.1002/ardp.19853180416

Reference yield: 85.0%

N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>dithiocarbamidsaeure (96924-45-7) + methyl iodide (74-88-4) → N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>dithiocarbamidsaeuremethylesterhydroiodid

Guidance literature:

In methanol; Ambient temperature;

DOI:10.1002/ardp.19853180416

Reference yield:

N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>dithiocarbamidsaeure (96924-45-7) → N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>-1,3,4-thiadiazol-2-amin

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / methanol / Ambient temperature

2: NH₂NH₂*H₂O / ethanol / 48 h

3: 54 percent / conc. HCl / ethanol / 8 h / Heating

With hydrogenchloride; hydrazine hydrate; In methanol; ethanol;

DOI:10.1002/ardp.19853180416

upstream raw materials:

carbon disulfide

N-<3-<3-(1-piperidinylmethyl)phenoxy>propyl>amine

Downstream raw materials:

2-(Phenylmethylen)-N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>hydrazincarbothioamid

N-<3-<3-(1-Piperidinylmethyl)phenoxy>propyl>hydrazincarbothioamid