(3S)-3-(3-Methoxy-4-methylphenyl)butan-2-ol

Base Information

Chemical Name:(3S)-3-(3-Methoxy-4-methylphenyl)butan-2-ol
CAS No.:97329-88-9
Molecular Formula:C₁₂H₁₈O₂
Molecular Weight:194.274
Hs Code.:

Synonyms:(3S)-3-(3-Methoxy-4-methylphenyl)butan-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S)-3-(3-Methoxy-4-methylphenyl)butan-2-ol

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Technology Process of (3S)-3-(3-Methoxy-4-methylphenyl)butan-2-ol

There total 15 articles about (3S)-3-(3-Methoxy-4-methylphenyl)butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 323195-90-0
(2E)-3-(3-Methoxy-4-methylphenyl)but-2-enal

: 97329-88-9
(3S)-3-(3-Methoxy-4-methylphenyl)butan-2-ol

Guidance literature:: With D-glucose; fermenting Baker's Yeast; resin XAD 1180; at 20 ℃; for 96h;
DOI:10.1039/b006141g

Reference yield:

: 1026505-57-6
(S)-4-tert-Butyl-2-[(S)-2-(3-methoxy-4-methyl-phenyl)-propyl]-4,5-dihydro-oxazole

: 97329-88-9
(3S)-3-(3-Methoxy-4-methylphenyl)butan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: aq. Na₂SO₄, TFA / tetrahydrofuran / 24 h / Ambient temperature

2: 1.) acetic anhydride, Py, 2.) LiAlH₄ / 1.) CH₂Cl₂, rt, 24 h, 2.) THF, 2 h

With pyridine; lithium aluminium tetrahydride; acetic anhydride; sodium sulfate; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1021/jo970429h

Reference yield:

: 586-30-1
3-hydroxy-4-methylbenzoic acid

: 97329-88-9
(3S)-3-(3-Methoxy-4-methylphenyl)butan-2-ol

Guidance literature:: Multi-step reaction with 9 steps

1.1: K₂CO₃ / acetone / 10 h / Heating

2.1: LiAlH₄ / tetrahydrofuran / 20 °C

3.1: MnO₂ / CHCl₃ / 3 h / Heating

4.1: tetrahydrofuran / 1 h / 0 °C

5.1: 15.9 g / MnO₂ / CHCl₃ / 4 h / Heating

6.1: NaH / tetrahydrofuran / 20 °C

6.2: 81 percent / tetrahydrofuran / 2 h / Heating

7.1: LiAlH₄ / tetrahydrofuran / 0 °C

8.1: MnO₂ / CHCl₃ / 6 h / Heating

9.1: 49 percent / resin XAD 1180; fermenting baker's yeast; aq. glucose / 96 h / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; D-glucose; fermenting Baker's Yeast; resin XAD 1180; sodium hydride; potassium carbonate; In tetrahydrofuran; chloroform; acetone; 6.2: Horner-Wadsworth-Emmons reaction;
DOI:10.1039/b006141g