(3S)-3-(3-Methoxy-4-methylphenyl)butyl iodide

Base Information

Chemical Name:(3S)-3-(3-Methoxy-4-methylphenyl)butyl iodide
CAS No.:323195-87-5
Molecular Formula:C₁₂H₁₇IO
Molecular Weight:304.171
Hs Code.:

Synonyms:(3S)-3-(3-Methoxy-4-methylphenyl)butyl iodide

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Chemical Property of (3S)-3-(3-Methoxy-4-methylphenyl)butyl iodide

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Technology Process of (3S)-3-(3-Methoxy-4-methylphenyl)butyl iodide

There total 11 articles about (3S)-3-(3-Methoxy-4-methylphenyl)butyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Toluene-4-sulfonic acid (S)-3-(3-methoxy-4-methyl-phenyl)-butyl ester

: 323195-87-5
(3S)-3-(3-Methoxy-4-methylphenyl)butyl iodide

Guidance literature:: With sodium iodide; In acetone; for 2h; Heating;
DOI:10.1039/b006141g

Reference yield:

: 7151-68-0
3-methoxy-p-toluic acid

: 323195-87-5
(3S)-3-(3-Methoxy-4-methylphenyl)butyl iodide

Guidance literature:: Multi-step reaction with 10 steps

1.1: LiAlH₄ / tetrahydrofuran / 20 °C

2.1: MnO₂ / CHCl₃ / 3 h / Heating

3.1: tetrahydrofuran / 1 h / 0 °C

4.1: 15.9 g / MnO₂ / CHCl₃ / 4 h / Heating

5.1: NaH / tetrahydrofuran / 20 °C

5.2: 81 percent / tetrahydrofuran / 2 h / Heating

6.1: LiAlH₄ / tetrahydrofuran / 0 °C

7.1: MnO₂ / CHCl₃ / 6 h / Heating

8.1: 49 percent / resin XAD 1180; fermenting baker's yeast; aq. glucose / 96 h / 20 °C

9.1: pyridine / CH₂Cl₂ / 5 h / 20 °C

10.1: NaI / acetone / 2 h / Heating

With pyridine; manganese(IV) oxide; lithium aluminium tetrahydride; D-glucose; fermenting Baker's Yeast; resin XAD 1180; sodium hydride; sodium iodide; In tetrahydrofuran; dichloromethane; chloroform; acetone; 5.2: Horner-Wadsworth-Emmons reaction;
DOI:10.1039/b006141g

Reference yield:

: 24973-22-6
3-methoxy-4-methylbenzaldehyde

: 323195-87-5
(3S)-3-(3-Methoxy-4-methylphenyl)butyl iodide

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran / 1 h / 0 °C

2.1: 15.9 g / MnO₂ / CHCl₃ / 4 h / Heating

3.1: NaH / tetrahydrofuran / 20 °C

3.2: 81 percent / tetrahydrofuran / 2 h / Heating

4.1: LiAlH₄ / tetrahydrofuran / 0 °C

5.1: MnO₂ / CHCl₃ / 6 h / Heating

6.1: 49 percent / resin XAD 1180; fermenting baker's yeast; aq. glucose / 96 h / 20 °C

7.1: pyridine / CH₂Cl₂ / 5 h / 20 °C

8.1: NaI / acetone / 2 h / Heating

With pyridine; manganese(IV) oxide; lithium aluminium tetrahydride; D-glucose; fermenting Baker's Yeast; resin XAD 1180; sodium hydride; sodium iodide; In tetrahydrofuran; dichloromethane; chloroform; acetone; 3.2: Horner-Wadsworth-Emmons reaction;
DOI:10.1039/b006141g